3,3',5,5'-四叔丁基-4,4'-联苯醌合成路线 (共 172 条)
反应条件
cyclohexane in pyridine 3 h; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 127, # 1 p. 267 - 270
反应条件
in various solvent(s) T=50°C; 1 h;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 45, # 10 p. 2675 - 2683
反应条件
1: 96.1 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.02 h / Ambient temperature 2: K3Fe(CN)6, KOH / benzene / 51 h / Ambient temperature View Scheme
参考文献
Heterocycles, , vol. 43, # 5 p. 941 - 944
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in benzene
参考文献
Justus Liebigs Annalen der Chemie, , vol. 645, p. 66 - 78
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in benzene
参考文献
Justus Liebigs Annalen der Chemie, , vol. 645, p. 66 - 78
反应条件
perchloric acid; cerium(IV) perchlorate in hexane; acetonitrile 0.333333 h; or electrochemical oxidation;
参考文献
Russian Journal of Physical Chemistry, , vol. 65, # 12 p. 1795 - 1798
Zhurnal Fizicheskoi Khimii, , vol. 65, p. 3387 - 3392
反应条件
potassium tert-butylate in tert-butyl alcohol T=30°C; concentration dependence; Rate constantProduct distribution;
参考文献
Journal of the American Chemical Society, , vol. 104, # 8 p. 2284 - 2290
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in benzene 24 h; Yield given;
参考文献
Liebigs Annales, , # 7 p. 1183 - 1186
反应条件
1: 1) PbO2; 2) 5percent NaOEt / 1) benzene; 1 h, room temp.; 2) EtOH, 1 h, reflux 2: 2.5 percent / PbO2 / benzene / 1 h / Ambient temperature View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 47, # 1+2 p. 7 - 13
反应条件
1: Mg, aq. NH4Cl / methanol / Heating 2: K3<Fe(CN)6>, aq. KOH / benzene View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 645, p. 66 - 78