3,3',5,5'-四叔丁基-4,4'-联苯醌合成路线 （共 172 条）
反应条件
in acetonitrile MoO2Cl2 soln. in CH3CN was added to LiO(2,6-t-Bu2C6H3) soln. in CH3CN and mixt. was stirred for 1 h; solvent was removed in vacuo, solved in pentane, filtered and placed in-35°C freezer for 2 days; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 39, # 4 p. 630 - 631
反应条件
1: [Ir2(OMe)2(1,5-cyclooctadiene)2]; 4,4'-di-tert-butyl-2,2'-dipyridyl / tetrahydrofuran / 40 h / 80 °C / |Inert atmosphere 2: dihydrogen peroxide; sodium hydroxide / methanol; tetrahydrofuran / 1 h / 0 °C / |Inert atmosphere 3: oxygen; (R,R)-Cr(salen)Cl / 1,2-dichloro-ethane / 17 h / 80 °C / |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 136, # 19 p. 6782 - 6785
反应条件
Mn(III) acetylacetonate in acetic acid 0.0166667 h; Heating; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 2 p. 620 - 622
反应条件
in dichloromethane 16 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 55, # 13 p. 4039 - 4043
参考文献
Journal of Organic Chemistry, , vol. 55, # 13 p. 4039 - 4043
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in chloroform; water
参考文献
Australian Journal of Chemistry, , vol. 33, # 2 p. 351 - 369
反应条件
dihydrogen peroxide; iodine in methanol T=35°C; 0.833333 h; other time 15 min; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 6 p. 2006 - 2012
反应条件
iodine in methanol; water T=35°C; 0.166667 h; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 61, # 6 p. 2006 - 2012
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in chloroform; water 0.0666667 h;
参考文献
Australian Journal of Chemistry, , vol. 33, # 2 p. 351 - 369
反应条件
in tert-butyl alcohol T=30°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 104, # 8 p. 2284 - 2290
