3,3',5,5'-四叔丁基-4,4'-联苯醌合成路线 (共 172 条)
反应条件
potassium hydroxide; iodine in methanol
参考文献
Journal of Organic Chemistry, , vol. 49, # 17 p. 3046 - 3050
反应条件
potassium tert-butylate in tert-butyl alcohol T=30°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 104, # 8 p. 2284 - 2290
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in benzene 51 h; Ambient temperature;
参考文献
Heterocycles, , vol. 43, # 5 p. 941 - 944
反应条件
1: 93 percent / diethyl ether / 2 h / 20 °C 2: 57 percent / MeLi / diethyl ether; tetrahydrofuran / -30 - 20 °C 3: 80 percent / PbO2 / various solvent(s) / 0.5 h / 20 °C View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 688, # 1-2 p. 192 - 199
反应条件
perchloric acid; lead dioxide; acetic acid in water
参考文献
Journal of Organic Chemistry, , vol. 73, # 3 p. 858 - 867
反应条件
(R,R)-Cr(salen)Cl; oxygen in 1,2-dichloro-ethane T=80°C; 17 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 136, # 19 p. 6782 - 6785
反应条件
in pyridine; cyclohexane 3 h; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 127, # 1 p. 267 - 270
反应条件
LiClO4-Pt in methanol; dichloromethane T=0 - 5°C; electrooxidation in divided and undivided cells with various ratio of solvents and with or without H2SO4 addn.; Product distribution;
参考文献
Tetrahedron Letters, , vol. 30, # 16 p. 2105 - 2108
反应条件
1: 55 percent / MeLi / diethyl ether; tetrahydrofuran / -30 - 20 °C 2: 98 percent / PbO2 / various solvent(s) / 20 °C View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 688, # 1-2 p. 192 - 199
反应条件
1: 57 percent / MeLi / diethyl ether; tetrahydrofuran / -30 - 20 °C 2: 80 percent / PbO2 / various solvent(s) / 0.5 h / 20 °C View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 688, # 1-2 p. 192 - 199