3-苄氧基-反-β-硝基苯乙烯合成路线 （共 13 条）
反应条件
ammonium acetate; acetic acid 2 h; Heating / reflux;
参考文献
Conte-Mayweg, Aurelia; Kuehne, Holger; Luebbers, Thomas; Maugeais, Cyrille; Mueller, Werner; Pflieger, Philippe
Patent: US2006/30613 A1, 2006 ;
Location in patent: Page/Page column 22 ;
反应条件
1: potassium carbonate / ethanol / 6 h / |Reflux 2: ammonium acetate / acetic acid / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 22 p. 6589 - 6597,9
反应条件
1: potassium carbonate / ethanol / 6 h / |Reflux 2: ammonium acetate / acetic acid / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 22 p. 6589 - 6597,9
反应条件
1: LAH / tetrahydrofuran 2: H2 / Pd/C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 1 p. 47 - 50
反应条件
lithium aluminium tetrahydride in diethyl ether; dichloromethane 0.5 h; Ambient temperature;
参考文献
Anderson, Wayne K.; McPherson, Howard L.; New, James S.; Rick, Arvela C.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 10 p. 1321 - 1325
反应条件
1: LAH / tetrahydrofuran 2: H2 / Pd/C 3: ethanol View Scheme
参考文献
Anderson, Wayne K.; McPherson, Howard L.; New, James S.; Rick, Arvela C.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 10 p. 1321 - 1325
反应条件
1: With lithium borohydride; chloro-trimethyl-silane in tetrahydrofuran T=20°C; 72.58 h; 2: With methanol in tetrahydrofuran 1 h; 3: With hydrogenchloride in diethyl ether 0.5 h;
参考文献
Conte-Mayweg, Aurelia; Kuehne, Holger; Luebbers, Thomas; Maugeais, Cyrille; Mueller, Werner; Pflieger, Philippe
Patent: US2006/30613 A1, 2006 ;
Location in patent: Page/Page column 22 ;
反应条件
dimethylsulfide; boron trifluoride diethyl etherate in dichloromethane T=30°C; 1.5 h;
参考文献
Fuji; Kawabata; Fujita
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 12 p. 3662 - 3664
反应条件
1: LAH / tetrahydrofuran 2: H2 / Pd/C 3: ethanol 4: HCl View Scheme
参考文献
Ma, Dawei; Wu, Wengen; Yang, Guoxin; Li, Jingya; Li, Jia; Ye, Qizhuang
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 1 p. 47 - 50
反应条件
1: 63 percent / LiAlH4 / tetrahydrofuran
2: 74 percent / triethylamine / diethyl ether / 1 h / Ambient temperature
3: 54 percent / dimethylformamide / 32 h / 100 °C
4: 59 percent / phosphorous oxychloride / benzene / 2 h / Heating
View Scheme
参考文献
Hocquaux; Marcot; Redeuilh; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 4 p. 319 - 329
