4-(二甲基氨基)-偶氮苯氯化物合成路线 （共 40 条）
反应条件
1: 2,4-di-Nitrobenzene With potassium borohydride in methanol; dimethyl sulfoxide T=0 - 3°C; Reduction; 0.666667 h; 2: 4-(N,N-dimethylaminophenyl)diazonium tetrafluoroborate in methanol; dimethyl sulfoxide Substitution; 0.5 h;
参考文献
Atroshchenko; Blokhina; Shakhkel'dyan; Grudtsyn; Gitis; Borbulevich; Blokhin; Kaminskii; Shishkin; Andrianov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 5 p. 684 - 692
反应条件
xanthone powder in acetonitrile T=20°C; Photolysis;
参考文献
Milanesi, Silvia; Fagnoni, Maurizio; Albini, Angelo
Chemical Communications, 2003 , # 2 p. 216 - 217
参考文献
Milanesi, Silvia; Fagnoni, Maurizio; Albini, Angelo
Chemical Communications, 2003 , # 2 p. 216 - 217
反应条件
C6H4N2O4(1-)*K(1+) in tetrahydrofuran T=-20°C; 1 h;
参考文献
Todres, Z. V.; Ovsepyan G. Ts.; Kosnikov, A. Yu.; Lindeman, S. V.; Struchkov, Yu. T.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 3.2 p. 522 - 527
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 3 p. 610 - 616
反应条件
in tetrahydrofuran T=-30°C; 1 h;
参考文献
Todres, Z. V.; Hovsepyan, G. TS.; Ionina, YE. A.
Tetrahedron, 1988 , vol. 44, # 16 p. 5199 - 5204
反应条件
in tetrahydrofuran T=-20°C; 1 h;
参考文献
Todres, Z. V.; Ovsepyan G. Ts.; Kosnikov, A. Yu.; Lindeman, S. V.; Struchkov, Yu. T.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 3.2 p. 522 - 527
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 3 p. 610 - 616
反应条件
1: 4-(N,N-dimethylaminophenyl)diazonium tetrafluoroborate With copper(I) isothiocyanate; sodium isothiocyanate; caesium carbonate in acetonitrile T=20°C; 0.166667 h; Inert atmosphere; 2: (trifluoromethyl)-trimethylsilane in acetonitrile T=20°C; 16 h; Inert atmosphere;
参考文献
Danoun, Gregory; Bayarmagnai, Bilguun; Gruenberg, Matthias F.; Goossen, Lukas J.
Chemical Science, 2014 , vol. 5, # 4 p. 1312 - 1316
反应条件
xanthone powder in acetonitrile T=20°C; Photolysis;
参考文献
Journal of Organic Chemistry, , vol. 70, # 2 p. 603 - 610
反应条件
xanthone powder in acetonitrile Irradiation;
参考文献
Chemical Communications, , # 2 p. 216 - 217
反应条件
C6H4N2O4(1-)*K(1+) in tetrahydrofuran T=-20°C; 1 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 26, # 3.2 p. 522 - 527
Zhurnal Organicheskoi Khimii, , vol. 26, # 3 p. 610 - 616
