反应条件
1: 9.6 g / boron trichloride / CH2Cl2 / 1 h / -10 °C
2: 8.25 g / zinc amalgam, conc. hydrochloric acid / acetic acid; H2O / 2 h / Heating
3: 1.) hydrobromic acid, 2.) potassium carbonate / 1.) glacial acetic acid, reflux, 18 h, 2.) DMF, 24 h
View Scheme
参考文献
Sargent, Melvyn V.; Stransky, Peter O.; Patrick, Vincent A.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 2 p. 231 - 239
