7-(4-叔丁基苯基)-2-甲基-1H-茚合成路线 (共 2 条)
反应条件
(IPr)NiCl2PPh3 in tetrahydrofuran T=20°C; 0.833333 h; Reflux;
参考文献
WO2013/7650 A1, ;
Page/Page column 54 ;
反应条件
1: 4-tert-butyl-2',3'-bis(chloromethyl)biphenyl With magnesium-anthracene in tetrahydrofuran T=0 - 20°C; 1 h; 2: methyl acetate in tetrahydrofuran T=0 - 20°C; 3: With toluene-4-sulfonic acid in toluene 1.5 h; Heating / reflux;
参考文献
WO2004/37756 A1, ;
Example 4 ;