1-氮杂螺[3.5]-2-壬酮合成路线 （共 8 条）
反应条件
sulfuric acid Heating;
参考文献
Suzuki, Takeshi; Imanishi, Naoki; Itahana, Hirotsune; Watanuki, Susumu; Miyata, Keiji; Ohta, Mitsuaki; Nakahara, Hideaki; Yamagiwa, Yoko; Mase, Toshiyasu
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 7 p. 1116 - 1124
反应条件
sodium dithionite; 15-crown-5; tetra-(n-butyl)ammonium iodide in N,N-dimethyl-formamide
336 h;
参考文献
Barrett, Anthony G. M.; Betts, Michael J.; Fenwick, Ashley
Journal of Organic Chemistry, 1985 , vol. 50, # 2 p. 169 - 175
反应条件
ammonium chloride; zinc in tetrahydrofuran; water
参考文献
Barrett, Anthony G. M.; Fenwick, Ashley; Betts, Michael J.
Journal of the Chemical Society, Chemical Communications, 1983 , # 6 p. 299 - 301
反应条件
magnesium silicate in diethyl ether
参考文献
Barrett, Anthony G. M.; Betts, Michael J.; Fenwick, Ashley
Journal of Organic Chemistry, 1985 , vol. 50, # 2 p. 169 - 175
反应条件
ammonium chloride; zinc in tetrahydrofuran; water
72 h;
参考文献
Barrett, Anthony G. M.; Betts, Michael J.; Fenwick, Ashley
Journal of Organic Chemistry, 1985 , vol. 50, # 2 p. 169 - 175
反应条件
1: diethyl ether / 0 °C
2: 1.15 g / Na2SO3, KOH / diethyl ether; H2O
View Scheme
参考文献
Palomo, Claudio; Oiarbide, Mikel; Bindi, Simona
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2469 - 2474
反应条件
potassium hydroxide; sodium sulfite in diethyl ether; water
参考文献
Palomo, Claudio; Oiarbide, Mikel; Bindi, Simona
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2469 - 2474
反应条件
potassium hydroxide; sodium thiosulfate
1.) ether, 30 min, RT, 2.) ether, 2 h; Yield given. Multistep reaction;
参考文献
Suzuki, Takeshi; Imanishi, Naoki; Itahana, Hirotsune; Watanuki, Susumu; Miyata, Keiji; Ohta, Mitsuaki; Nakahara, Hideaki; Yamagiwa, Yoko; Mase, Toshiyasu
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 7 p. 1116 - 1124
