N-乙酰基-L-苏氨酸甲酯合成路线 （共 5 条）
反应条件
1.1: Et3N / methanol 2.1: NBS / CH2Cl2 2.2: Et3N / CH2Cl2 View Scheme
参考文献
Roff, Geoffrey J.; Lloyd, Richard C.; Turner, Nicholas J.
Journal of the American Chemical Society, 2004 , vol. 126, # 13 p. 4098 - 4099
反应条件
in acetonitrile T=32°C; 20 h; Irradiation;
参考文献
Deseke, Eckart; Nakatani, Yoichi; Ourisson, Guy
European Journal of Organic Chemistry, 1998 , # 2 p. 243 - 251
反应条件
1.1: Et3N / methanol
2.1: NBS / CH2Cl2
2.2: Et3N / CH2Cl2
View Scheme
参考文献
Roff, Geoffrey J.; Lloyd, Richard C.; Turner, Nicholas J.
Journal of the American Chemical Society, 2004 , vol. 126, # 13 p. 4098 - 4099
反应条件
1.1: Et3N / methanol
2.1: NIS; TFA / CH2Cl2 / 20 °C
2.2: 40 percent / Et3N / CH2Cl2 / 1 h
View Scheme
参考文献
KUNG, Hank, F.; CHOI, Seok, Rye; HAN, Guoxia
Patent: WO2007/1466 A2, 2007 ;
Location in patent: Page/Page column 22-23 ;
WO 2007/001466 A2
反应条件
1.1: Et3N / methanol
2.1: NIS; TFA / CH2Cl2 / 20 °C
2.2: 40 percent / Et3N / CH2Cl2 / 1 h
3.1: 81 percent / Pd(OAc)2; Na2CO3 / ethanol / 4 h / 55 °C
View Scheme
参考文献
Roff, Geoffrey J.; Lloyd, Richard C.; Turner, Nicholas J.
Journal of the American Chemical Society, 2004 , vol. 126, # 13 p. 4098 - 4099
