2-(2-甲氧基苯基)-1,3-二噻烷合成路线 (共 6 条)
反应条件
boron trifluoride diethyl etherate in dichloromethane 20 h; Ambient temperature;
参考文献
Shaterian, Hamid Reza; Azizi, Kobra; Fahimi, Nafiseh
Journal of Sulfur Chemistry, 2011 , vol. 32, # 1 p. 85 - 91
反应条件
iodine in chloroform T=20°C; 0.25 h;
参考文献
Firouzabadi; Iranpoor; Hazarkhani
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7527 - 7529
反应条件
lithium trifluoromethane sulfonate T=90°C; 4 h;
参考文献
Firouzabadi, Habib; Eslami, Shahram; Karimi, Babak
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 12 p. 2401 - 2406
反应条件
1.1: n-BuLi / hexane; tetrahydrofuran / 1 h / -23 °C 1.2: 90 percent / hexane; tetrahydrofuran / 1 h / 0 °C 2.1: 65 percent / HgCl2; water; CaCO3 / acetone / 20 °C 3.1: baker's yeast on montmorillonite K10; 2 percent aq. KCl; sucrose / 48 h / 35 °C / Enzymatic reaction View Scheme
参考文献
Patrocinio, Amauri F.; Correa Jr., Ivan R.; Moran, Paulo J. S.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 21 p. 3133 - 3137
反应条件
p-benozquinone; sodium iodide in water; acetonitrile T=100°C; 24 h;
参考文献
Inamoto, Kiyofumi; Yamada, Tetsuya; Kato, Sei-Ichi; Kikkawa, Shoko; Kondo, Yoshinori
Tetrahedron, 2013 , vol. 69, # 44 p. 9192 - 9199
反应条件
1.1: n-BuLi / hexane; tetrahydrofuran / 1 h / -23 °C 1.2: 90 percent / hexane; tetrahydrofuran / 1 h / 0 °C 2.1: 65 percent / HgCl2; water; CaCO3 / acetone / 20 °C 3.1: 30 percent / baker's yeast on montmorillonite K10; 2 percent aq. KCl; sucrose / 48 h / 35 °C / Enzymatic reaction View Scheme
参考文献
Patrocinio, Amauri F.; Correa Jr., Ivan R.; Moran, Paulo J. S.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 21 p. 3133 - 3137