4-甲氧基苯甲醛三亚甲基二硫代缩醛合成路线 （共 28 条）
反应条件
sodium nitrate; sulfuric acid; silica gel in dichloromethane T=20°C; 0.166667 h;
参考文献
Synthesis, , # 9 p. 1480 - 1484
反应条件
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene T=20°C; 2 h;
参考文献
Synlett, , # 10 p. 1686 - 1690
反应条件
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene in methanol T=20°C; 4 h;
参考文献
Ichige, Takahiro; Miyake, Annu; Kanoh, Naoki; Nakata, Masaya
Synlett, 2004 , # 10 p. 1686 - 1690
反应条件
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene T=20°C; 2 h;
参考文献
Synlett, , # 10 p. 1686 - 1690
反应条件
bismuth(III) chloride; benzyltriphenylphosphonium peroxymonosulfate in acetonitrile 3 h; Heating;
参考文献
Hajipour; Mallakpour; Mohammadpoor-Baltork; Adibi
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2805 - 2811
反应条件
1.1: n-butyllithium / tetrahydrofuran / -40 - -20 °C / |Inert atmosphere 1.2: 3 h / -78 °C / |Inert atmosphere 2.1: 18-crown-6 ether / dimethyl sulfoxide / 4 h / 100 °C / |Inert atmosphere 3.1: iodine; sodium hydrogencarbonate; water / acetone / 2 h / 0 °C View Scheme
参考文献
Franz, Sarah E.; Watkins, Richard R.; Wright, Laura A.; Weaver, Blair A.; Hartage, Ramon C.; Ghiviriga, Ion; Gumina, Giuseppe; Feske, Brent D.
Synthesis (Germany), 2013 , vol. 45, # 15 art. no. SS-2013-M0268-OP, p. 2171 - 2178
反应条件
H3[PW12O40] in Petroleum ether
0.0166667 h; Heating;
参考文献
Farago, Janos; Kotschy, Andras
Synthesis, 2009 , # 1 p. 85 - 90
反应条件
iodine in chloroform
T=20°C; 0.25 h;
参考文献
Firouzabadi; Iranpoor; Hazarkhani
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7527 - 7529
反应条件
Cu(DS)2 in water
T=20°C; 0.0833333 h; Inert atmosphere;
参考文献
Weng, Shiue-Shien; Chang, Shen-Chun; Chang, Tsuan-Hao; Chyn, Jong-Pyng; Lee, Shu-Wei; Lin, Chao-An; Chen, Fong-Kuang
Synthesis, 2010 , # 9 art. no. F23009SS, p. 1493 - 1499
反应条件
trichloroisocyanuric acid in chloroform
T=20°C; 1.5 h;
参考文献
Firouzabadi; Iranpoor; Hazarkhani
Synlett, 2001 , # 10 p. 1641 - 1643
