4-甲氧基苯甲醛三亚甲基二硫代缩醛合成路线 （共 28 条）
反应条件
in methanol
2.66667 h; Heating;
参考文献
Liu, Qun; Che, Guangbo; Yu, Haifeng; Liu, Yingchun; Zhang, Jingping; Zhang, Qian; Dong, Dewen
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 9148 - 9150
反应条件
1: 95 percent / solid silica chloride / acetonitrile / 20 °C
2: 94 percent / solid silica chloride / CHCl3 / 0.17 h / 20 °C
View Scheme
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
反应条件
1: sodium iodide; p-benozquinone / acetonitrile; water / 24 h / 100 °C
2: copper(II) sulfate / dichloromethane / 20 °C
View Scheme
参考文献
Inamoto, Kiyofumi; Yamada, Tetsuya; Kato, Sei-Ichi; Kikkawa, Shoko; Kondo, Yoshinori
Tetrahedron, 2013 , vol. 69, # 44 p. 9192 - 9199
反应条件
1: sodium iodide; p-benozquinone / acetonitrile; water / 48 h / 100 °C
2: copper(II) sulfate / dichloromethane / 20 °C
View Scheme
参考文献
Inamoto, Kiyofumi; Yamada, Tetsuya; Kato, Sei-Ichi; Kikkawa, Shoko; Kondo, Yoshinori
Tetrahedron, 2013 , vol. 69, # 44 p. 9192 - 9199
反应条件
in acetonitrile-D3
T=28°C; Rate constant;
参考文献
Stahl, Ingfried
Chemische Berichte, 1985 , vol. 118, # 12 p. 4857 - 4868
反应条件
1: 1.) BuLi / 1.) THF, hexane, -25 deg C, 2 h, 2.) THF, hexane, RT, overnight
2: 70 percent / 90percent aq.-methanolic chloramine T hydrate / ethanol / 1 h
View Scheme
参考文献
Inamoto, Kiyofumi; Yamada, Tetsuya; Kato, Sei-Ichi; Kikkawa, Shoko; Kondo, Yoshinori
Tetrahedron, 2013 , vol. 69, # 44 p. 9192 - 9199
反应条件
1: 1.) n-BuLi / 1.) TMEDA, -78 deg C, 2.) THF, -78 deg C, overnight
2: 72.8 percent / CF3COOH, 35 percent aq CH2O / CHCl3 / 72 h / Ambient temperature
View Scheme
参考文献
Yamamori, Teruo; Adachi, Ikuo
Tetrahedron Letters, 1980 , vol. 21, p. 1747 - 1750
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
