N-甲基-N-(三甲基硅烷基)三氟乙酰胺合成路线 （共 21 条）
反应条件
in acetonitrile 18 h; Heating;
参考文献
Millar, Ross W.; Philbin, Simon P.
Tetrahedron, 1997 , vol. 53, # 12 p. 4371 - 4386
反应条件
in dichloromethane; N,N-dimethyl-formamide; acetonitrile -78 degC, 4 h, -45 degC, 6 h; Title compound not separated from byproducts;
参考文献
Tyrra, Wieland; Naumann, Dieter
Journal of Fluorine Chemistry, 1989 , vol. 45, p. 401 - 416
反应条件
1: methanol; 2-(4-hydroxy-3-methoxyphenyl)-2-methoxyacetonitrile With manganese(IV) oxide; water 24 h; 2: N-methyl-N-(trimethylsilyl)-trifluoroacetamide Further stages.;
参考文献
Kindler, Bernhard L. J.; Spiteller, Peter
Angewandte Chemie - International Edition, 2007 , vol. 46, # 42 p. 8076 - 8078
反应条件
in dichloromethane; N,N-dimethyl-formamide; acetonitrile -78 degC, 4 h, -45 degC, 6 h; Title compound not separated from byproducts;
参考文献
Tyrra, Wieland; Naumann, Dieter
Journal of Fluorine Chemistry, 1989 , vol. 45, p. 401 - 416
反应条件
chloro-trimethyl-silane T=25°C; 2 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 68, # 1-4 p. 25 - 36
反应条件
in acetonitrile 18 h; Heating;
参考文献
Millar, Ross W.; Philbin, Simon P.
Tetrahedron, 1997 , vol. 53, # 12 p. 4371 - 4386
参考文献
Thoma, Heinz; Spiteller, Gerhard
Liebigs Annalen der Chemie, 1983 , # 7 p. 1237 - 1248
反应条件
3 h; Ambient temperature;
参考文献
Staubmann, Ruth; Schubert-Zsilavecz, Manfred; Hiermann, Alois; Kartnig, Theodor
Phytochemistry, 1999 , vol. 50, # 2 p. 337 - 338
反应条件
in tetrahydrofuran 12 h; Ambient temperatureor 60 deg C, 30 min;
参考文献
Kraus, Rupert; Spiteller, Gerhard
Phytochemistry (Elsevier), 1990 , vol. 29, # 5 p. 1653 - 1659
反应条件
T=60°C; 1 h; Inert atmosphere;
参考文献
Kelley, Paul; Lin, Sibo; Edouard, Guy; Day, Michael W.; Agapie, Theodor
Journal of the American Chemical Society, 2012 , vol. 134, # 12 p. 5480 - 5483
