1,2,4-苯三羧酸三甲酯合成路线 (共 45 条)
反应条件
triphenylphosphine; bis(1,5-cyclooctadiene)nickel (0) in tetrahydrofuran T=20°C; Product distribution; Further Variations:Catalysts;
参考文献
Chemical Communications, , # 2 p. 181 - 182
反应条件
(CO)3Ni(PPh3)2 in benzene 2 h; Heating; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Chemical Research, Miniprint, , # 8 p. 2201 - 2228
反应条件
(CO)3Ni(PPh3)2 in benzene 2 h; Heating; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Chemical Research, Miniprint, , # 8 p. 2201 - 2228
参考文献
Neunhoeffer, Hans; Werner, Gebhard
Liebigs Annalen der Chemie, 1985 , # 4 p. 853 - 856
反应条件
in n-heptane The soln. was refluxed for two hours under N2; separated by column chromy.. Recrystn. from hexane/diethyl ether at -80°C yielded brown crystals. Detected by IR, NMR, Elem. anal.;
参考文献
Muller, Fred; Koten, Gerard van; Vrieze, Kees; Heijdenrijk, Dick; Krijnen, Bert B.; Stam, Casper H.
Organometallics, 1989 , vol. 8, p. 41 - 48
反应条件
2: sulfuric acid View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 31, p. 1297
反应条件
1: aqueous HCl; aqueous NaNO2 2: aqueous NaOH View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 21, p. 1648
反应条件
1: aqueous NaOH View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 21, p. 1648
反应条件
in toluene the mixt. in toluene was heated at 70°C for 24 h; solvent was removed, not sepd., detected by NMR spectra;
参考文献
Organometallics, , vol. 19, # 21 p. 4289 - 4294
反应条件
in chloroform the mixt. in CHCl3 was heated at reflux for 24 h; solvent was removed, not sepd., detected by NMR spectra;
参考文献
Organometallics, , vol. 19, # 21 p. 4289 - 4294