5-苯基-4-戊炔-1-醇合成路线 (共 19 条)
反应条件
2: KOH / aq. ethanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 37, # 17 p. 2782 - 2784
反应条件
1: Li, liq. NH3 2: NaI / acetone 4: KOH / aq. ethanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 37, # 17 p. 2782 - 2784
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide T=60°C; Sonogashira Cross-Coupling; 16 h; Schlenk techniqueInert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 2 p. 427 - 437
反应条件
boron trifluoride diethyl etherate
参考文献
Helvetica Chimica Acta, , vol. 86, # 3 p. 865 - 893
参考文献
Bulletin de la Societe Chimique de France, , p. 1084 - 1089
反应条件
chromium(VI) oxide; sulfuric acid in acetone T=5 - 20°C; 4 h;
参考文献
Abbiati, Giorgio; Contini, Alessandro; Nava, Donatella; Rossi, Elisabetta
Tetrahedron, 2009 , vol. 65, # 24 p. 4664 - 4670
反应条件
pyridinium chlorochromate in dichloromethane
参考文献
Wessig, Pablo; Muehling, Olaf
Helvetica Chimica Acta, 2003 , vol. 86, # 3 p. 865 - 893
反应条件
1: 99 percent / LAH / tetrahydrofuran / 20 h / Heating
2: 95 percent / imidazole / dimethylformamide / 0 - 20 °C
3: 72 percent / m-CPBA; NaOAc / CH2Cl2 / 6 h / 20 °C
View Scheme
参考文献
Seiders II, John R.; Wang, Lijun; Floreancig, Paul E.
Journal of the American Chemical Society, 2003 , vol. 125, # 9 p. 2406 - 2407
反应条件
1: lithium aluminium tetrahydride
View Scheme
参考文献
Schmidt, Valerie A.; Alexanian, Erik J.
Journal of the American Chemical Society, 2011 , vol. 133, # 30 p. 11402 - 11405