4,4’-双(2,3-环氧基丙氧基)联苯合成路线 (共 3 条)
反应条件
1: 4,4'-Dihydroxybiphenyl With sodium hydride in N,N-dimethyl-formamide 0.166667 h; Inert atmosphere; 2: epichlorohydrin in N,N-dimethyl-formamide T=20°C; 48 h; Inert atmosphere; 3: With water in N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
BRITISH COLUMBIA CANCER AGENCY BRANCH; THE UNIVERSITY OF BRITISH COLUMBIA; SADAR, Marianne D.; MAWJI, Nasrin R.; BANUELOS, Carmen Adriana; ANDERSEN, Raymond J.; GARCIA FERNANDEZ, Javier
Patent: WO2011/82488 A1, 2011 ;
Location in patent: Page/Page column 97-98 ;
反应条件
sodium sulfate; methyloxirane; potassium hydroxide in chloroform
参考文献
The Dow Chemical Company
Patent: US5362822 A1, 1994 ;
反应条件
potassium hydroxide T=20°C; Title compound not separated from byproducts;
参考文献
Sharma; Bala, Madhu
Journal of the Indian Chemical Society, 2005 , vol. 82, # 11 p. 975 - 977