1,4-二(4-溴苯基)丁烷-1,4-二酮合成路线 (共 22 条)
反应条件
iodine; zinc in tetrahydrofuran
16 h; Heating;
参考文献
Ceylan, Mustafa; Guerdere, M. Burcu; Budak, Yakup; Kazaz, Cavit; Secen, Hasan
Synthesis, 2004 , # 11 p. 1750 - 1754
反应条件
indium monobromide in tetrahydrofuran
T=20°C; 24 h;
参考文献
Peppe, Clovis; Pavao Das Chagas, Rafael
Synlett, 2004 , # 7 p. 1187 - 1190
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O; potassium carbonate; triethylamine in acetonitrile
T=20°C; 16 h; Schlenk techniqueIrradiation;
参考文献
Xuan, Jun; Feng, Zhu-Jia; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing
Chemistry - A European Journal, 2014 , vol. 20, # 11 p. 3045 - 3049
反应条件
titanium(IV) isopropylate in tetrachloromethane
T=20°C; 168 h;
参考文献
Kulinkovich, O. G.; Kel'in, A. V.; Senin, P. V.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 8 p. 1060 - 1062
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 8 p. 1166 - 1168
反应条件
indium monobromide in tetrahydrofuran
T=20°C; 24 h;
参考文献
Peppe, Clovis; Pavao Das Chagas, Rafael
Synlett, 2004 , # 7 p. 1187 - 1190
参考文献
ABBOTT LABAORATORIES
Patent: US2010/317568 A1, 2010 ;
反应条件
methanol; Woollins’ reagent
T=20°C; 2 h; chemoselective reaction;
参考文献
Mandal, Madhumita; Chatterjee, Sourav; Jaisankar, Parasuraman
Synlett, 2012 , vol. 23, # 18 p. 2615 - 2618,4
反应条件
aluminum isopropoxide; isopropyl alcohol
参考文献
Lutz; Gillespie
Journal of the American Chemical Society, 1950 , vol. 72, p. 344
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Campbell; Khanna
Nature (London, United Kingdom), 1948 , vol. 161, p. 54
反应条件
methanol; Woollins’ reagent
T=20°C; 2 h; chemoselective reaction;
参考文献
Mandal, Madhumita; Chatterjee, Sourav; Jaisankar, Parasuraman
Synlett, 2012 , vol. 23, # 18 p. 2615 - 2618,4
反应条件
2: bromine
3: alcohol
4: aqueous alcoholic KOH-solution
View Scheme
参考文献
Hale; Thorp
Journal of the American Chemical Society, 1913 , vol. 35, p. 267