3,3'-二硫代二[6-羟基-苯甲酸]合成路线 （共 5 条）
反应条件
hydrogenchloride; tin in water Cooling with iceReflux;
参考文献
Li, Jin-Ling; Gao, Zi-Wei; Sun, Ping; Gao, Ling-Xiang; Tikkanen, Wayne
Inorganica Chimica Acta, 2011 , vol. 368, # 1 p. 231 - 236
反应条件
1.1: sodium hydroxide; sodium nitrite / water / 5 °C 1.2: 5 °C 1.3: 1 h / 20 °C / |Inert atmosphere 2.1: potassium hydroxide / ethanol / 5 h View Scheme
参考文献
Saphier, Sigal; Haft, Avital; Margel, Shlomo
Journal of Medicinal Chemistry, 2012 , vol. 55, # 23 p. 10781 - 10785
参考文献
Kaufmann; Rossbach
Chemische Berichte, 1925 , vol. 58, p. 1558
反应条件
1: chlorosulfonic acid 2: zinc-dust; alcohol; concentrated aqueous HCl / anschl. mit Eisenchlorid und HCl View Scheme
参考文献
Stewart
Journal of the Chemical Society, 1922 , vol. 121, p. 2558
反应条件
2: zinc-dust; alcohol; concentrated aqueous HCl / anschl. mit Eisenchlorid und HCl View Scheme
参考文献
Stewart
Journal of the Chemical Society, 1922 , vol. 121, p. 2558
