反应条件
in neat (no solvent) heating of 0.5 g ZrBr3 in an evacuated pyrex glass tube at 350°C, 10-15 hours or at 390°C, 6 hours; temp. should be lower than 400°C;; removal of ZrBr4;;
参考文献
Fast, J. D.
Z. Anorg. Chem., 1939 , vol. 239, p. 145 - 154
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Young, R. C.
Journal of the American Chemical Society, 1931 , vol. 53, p. 2148 - 2153
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Young, R. C.
Journal of Chemical Education, 1943 , vol. 20, p. 378 - 378
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Young, R. C.
Journal of Chemical Education, 1943 , vol. 20, p. 380 - 380
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Gmelin Handbook: Zr: MVol., 121, page 314 - 315