(S)-(+)-1,3-丁二醇合成路线 (共 31 条)
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 1 h;
参考文献
Mohr, Peter; Roesslein, Lukas; Tamm, Christoph
Helvetica Chimica Acta, 1987 , vol. 70, p. 142 - 152
反应条件
phosphate buffer T=30°C; 24 h; Candida boidinii KK912 (IFO 10574);
参考文献
Chemistry Letters, , # 2 p. 251 - 254
反应条件
lithium aluminium tetrahydride in diethyl ether 8 h; Heating; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 47, # 20 p. 3850 - 3854
反应条件
phosphate buffer; pKK-CPA1 in water T=30°C; Isomerization; pH=6.5; 24 h;
参考文献
Bioscience, Biotechnology and Biochemistry, , vol. 63, # 6 p. 1051 - 1055
反应条件
toluene-4-sulfonic acid in methanol Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 57, # 5 p. 1412 - 1421
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Tetrahedron Letters, , vol. 40, # 21 p. 4093 - 4096
反应条件
potassium carbonate; (R,R)-iPrDuPhos 1) CH2Cl2, 2 h, 20-25 deg C, 2) MeOH, 4 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 33, # 16 p. 2099 - 2102
反应条件
hydrogenchloride; sodium nitrite
参考文献
Journal of Biological Chemistry, , vol. 69, p. 573
反应条件
lithium aluminium tetrahydride
参考文献
Tetrahedron Letters, , vol. 24, # 3 p. 287 - 290
反应条件
barium dihydroxide; methanesulfonic acid 1) MeOH, 16 h, reflux, 2) MeOH, 4 h, reflux; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 33, # 37 p. 5323 - 5326