2-羟基-3,5-二甲基-苯甲醛合成路线 （共 16 条）
反应条件
triethylamine; magnesium chloride in acetonitrile 3 h; Heating;
参考文献
Knight, Paul D.; O'Shaughnessy, Paul N.; Munslow, Ian J.; Kimberley, Brian S.; Scott, Peter
Journal of Organometallic Chemistry, 2003 , vol. 683, # 1 p. 103 - 113
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; sulfuric acid; acetic acid; paraformaldehyde in water
参考文献
Adir et Compagnie
Patent: US5391569 A1, 1995 ;
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; formaldehyd; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; toluene T=4 - 20°C; 52 h; Heating / reflux;
参考文献
PHARMACIA CORPRATION
Patent: WO2004/60376 A1, 2004 ;
Location in patent: Page/Page column 165-166 ;
反应条件
oxygen; iron(III) chloride; iron in methanol T=20°C; P=760 Torr; 72 h;
参考文献
Sparfel, Daniel; Baranne-Lafont, Joele; Cuong, Nguyen Kim; Capdevielle, Patrice; Maumy, Michel
Tetrahedron, 1990 , vol. 46, # 3 p. 793 - 802
反应条件
oxygen; copper; iron(II) chloride in methanol T=20°C; P=760 Torr; 72 h;
参考文献
Sparfel, Daniel; Baranne-Lafont, Joele; Cuong, Nguyen Kim; Capdevielle, Patrice; Maumy, Michel
Tetrahedron, 1990 , vol. 46, # 3 p. 793 - 802
反应条件
oxygen; iron(III) chloride; iron T=20°C; P=760 Torr; 72 h;
参考文献
Sparfel, Daniel; Baranne-Lafont, Joele; Cuong, Nguyen Kim; Capdevielle, Patrice; Maumy, Michel
Tetrahedron, 1990 , vol. 46, # 3 p. 793 - 802
反应条件
titanium tetrachloride in dichloromethane T=0°C; 12 h;
参考文献
Meier, Chris; Lorey, Martina; De Clercq, Eric; Balzarini, Jan
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1303 - 1306
反应条件
1: With acetic acid T=120 - 130°C; 2 h; 2: With sulfuric acid T=110°C; 3 h; Further stages.;
参考文献
Nomura, Nobuyoshi; Aoyama, Takuji; Ishii, Ryohei; Kondo, Tadao
Macromolecules, 2005 , vol. 38, # 13 p. 5363 - 5366
反应条件
tin(ll) chloride in 1,4-dioxane Heating;
参考文献
Sinhababu, Achintya K.; Borchardt, Ronald T.
Synthetic Communications, 1983 , vol. 13, # 8 p. 677 - 684
参考文献
Zinke; Pucher
Monatshefte fuer Chemie, 1948 , vol. 79, p. 26,36
