2-羟基-3,5-二甲基-苯甲醛合成路线 （共 16 条）
参考文献
Zigeuner; Jellinek
Monatshefte fuer Chemie, 1959 , vol. 90, p. 297,301
反应条件
T=160 - 170°C; Erhitzen im Kohlendioxyd-Strom, zuletzt unter 20 Torr;
参考文献
Zinke; Ziegler
Chemische Berichte, 1944 , vol. 77/79, p. 264,271
Chemische Berichte, 1941 , vol. 74, p. 541,545
参考文献
Hultzsch
Chemische Berichte, 1941 , vol. 74, p. 904,1539, 1542
反应条件
1: 3,5-dimethyl-2-hydroxybenzaldehyde With potassium carbonate in N,N-dimethyl-formamide T=20°C; 0.25 h; Inert atmosphere; 2: methyl iodide in N,N-dimethyl-formamide T=20°C; 12 h; Inert atmosphere;
参考文献
Fernandes, Rodney A.; Chowdhury, Asim K.
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8826 - 8829
反应条件
1: aqueous ethanol
2: zinc; ethanol; acetic acid
3: 280 °C / unter Kohlendioxyd
View Scheme
参考文献
Zinke; Pucher
Monatshefte fuer Chemie, 1948 , vol. 79, p. 26,36
反应条件
hydrogenchloride in methanol
T=20°C; Condensation; 48 h;
参考文献
Dinger, Maarten B.; Scott, Michael J.
European Journal of Organic Chemistry, 2000 , # 13 p. 2467 - 2478
