3-碘-2-苯基-苯并呋喃合成路线 （共 12 条）
反应条件
iodine cloride in dichloromethane
T=25°C; 3 h;
参考文献
Yue, Dawei; Yao, Tuanli; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 25 p. 10292 - 10296
反应条件
boron trifluoride diethyl etherate; bis(sym-collidine)iodine(I) hexafluorophosphate in dichloromethane
T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Okitsu, Takashi; Nakazawa, Daisuke; Taniguchi, Rie; Wada, Akimori
Organic Letters, 2008 , vol. 10, # 21 p. 4967 - 4970
反应条件
iodine in water
T=20°C; Green chemistry;
参考文献
Han, Jiang-Sheng; Shao, Yin-Lin; Zhang, Xiao-Hong; Zhong, Ping
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 11 p. 1599 - 1610
反应条件
1: phenylacetylene With n-butyllithium; boric acid trimethyl ester in ethylene glycol dimethyl ether; hexane
T=-78 - 20°C; 1.75 h;
2: 1-iodo-2-methoxybenzene With triphenylphosphine; palladium diacetate in ethylene glycol dimethyl ether
4 h; Heating;
3: With N-iodo-succinimide; boron trichloride in hexane; dichloromethane
T=20°C;
参考文献
Colobert, Francoise; Castanet, Anne-Sophie; Abillard, Olivier
European Journal of Organic Chemistry, 2005 , # 15 p. 3334 - 3341
反应条件
iodine; sodium hydrogencarbonate in acetonitrile
T=20°C; Iodination; 2 h;
参考文献
Arcadi, Antonio; Cacchi, Sandro
Synlett, 1999 , # 9 p. 1432 - 1434
反应条件
N-iodo-succinimide; trimethylsilylazide in 1,2-dichloro-ethane; acetonitrile
T=20 - 70°C; 3 h;
参考文献
Okamoto, Noriko; Ishikura, Minoru; Yanada, Reiko
Organic Letters, 2013 , vol. 15, # 11 p. 2571 - 2573
反应条件
copper(l) iodide; oxygen in N,N-dimethyl-formamide
T=135 - 140°C; 16 h;
参考文献
Swamy, Nalivela Kumara; Yazici, Arife; Pyne, Stephen G.
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3412 - 3419
反应条件
1: Et3N; CuI / PdCl2(PPh3)2 / 25 °C
2: 98 percent / ICl / CH2Cl2 / 3 h / 25 °C
View Scheme
参考文献
Yue, Dawei; Yao, Tuanli; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 25 p. 10292 - 10296
反应条件
iodine; palladium dichloride in acetonitrile
T=80°C; 36 h; Inert atmosphere;
参考文献
Du, Hui-Ai; Zhang, Xing-Guo; Tang, Ri-Yuan; Li, Jin-Heng
Journal of Organic Chemistry, 2009 , vol. 74, # 20 p. 7844 - 7848
反应条件
copper(l) iodide; oxygen in N,N-dimethyl-formamide
T=135 - 140°C; 16 h;
参考文献
Swamy, Nalivela Kumara; Yazici, Arife; Pyne, Stephen G.
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3412 - 3419
