3-氨基-2,6-哌啶二酮盐酸盐合成路线 (共 7 条)
反应条件
1: AcOH / Heating 2: H2 / 10 percent Pd/C / acetone / 2585.74 - 3102.89 Torr View Scheme
参考文献
Muller, George W.; Chen, Roger; Huang, Shaei-Yun; Corral, Laura G.; Wong, Lu Min; Patterson, Rebecca T.; Chen, Yuxi; Kaplan, Gilla; Stirling, David I.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 11 p. 1625 - 1630
反应条件
acetic acid Heating;
参考文献
Muller, George W.; Chen, Roger; Huang, Shaei-Yun; Corral, Laura G.; Wong, Lu Min; Patterson, Rebecca T.; Chen, Yuxi; Kaplan, Gilla; Stirling, David I.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 11 p. 1625 - 1630
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20 - 45°C; Product distribution / selectivity;
参考文献
RANBAXY LABORATORIES LIMITED; KAPOOR, Munish; KUMAR, Saridi, Madhava, Dileep; MURUGESAN, Balaguru; SATHYANARAYANA, Swargam; THAPER, Rajesh, Kumar; PRASAD, Mohan
Patent: WO2011/27326 A1, 2011 ;
Location in patent: Page/Page column 11 ;
反应条件
1: Et3N / dimethylformamide / 80 °C 2: H2 / 10 percent Pd/C / methanol View Scheme
参考文献
RATIOPHARM GMBH; STIEGEL, Hans-Huenter^, Dr.; ALBRECHT, Wolfgang, Dr.; BRUECK, Sandra; PAETZ, Jana; MEERGANS, Dominique
Patent: WO2011/50962 A1, 2011 ;
反应条件
1: in acetonitrile 0.25 h; 2: With triethylamine in water; acetonitrile T=15 - 87°C; 49.0833 - 50.8333 h; Product distribution / selectivity;
参考文献
Celgene Corporation an orgnization of the state New Jersey
Patent: US2007/4920 A1, 2007 ;
Location in patent: Page/Page column 13 ;
反应条件
1: AcOH / Heating 2: H2 / 10 percent Pd/C / acetone / 2585.74 - 3102.89 Torr View Scheme
参考文献
Muller, George W.; Chen, Roger; Huang, Shaei-Yun; Corral, Laura G.; Wong, Lu Min; Patterson, Rebecca T.; Chen, Yuxi; Kaplan, Gilla; Stirling, David I.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 11 p. 1625 - 1630
反应条件
sodium acetate in acetic acid
17 h; Heating / reflux;
参考文献
Celgene Corporation
Patent: US6335/349 B1, 2002 ;
Location in patent: Example 2 ;
Title/Abstract Full Text Show Details
Celgene Corporation
Patent: US6335349 B1, 2002 ;
Location in patent: Example 2 ;