1,1,1,5-四氯戊烷合成路线 （共 31 条）
反应条件
2,2'-azo-bisisobutyronitrile
参考文献
Joyce; Hanford; Harmon
Journal of the American Chemical Society, 1948 , vol. 70, p. 2531
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2440800 , 1942 ;
反应条件
anhydrous diethylamine hydrochloride; 1,2-diphenyl-2-hydroxyethanone; iron(III) chloride in isopropyl alcohol Further byproducts given;
参考文献
Moore,L.O.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2633 - 2635
反应条件
1,2-diphenyl-2-hydroxyethanone; diethylamine; iron(III) chloride in isopropyl alcohol Further byproducts given;
参考文献
Moore,L.O.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2633 - 2635
反应条件
chlorine in tetrachloromethane T=25°C; Irradiation;
参考文献
Burton,T.; Bruylants,A.
Bulletin des Societes Chimiques Belges, 1972 , vol. 81, p. 639 - 642
反应条件
1: AcOH, aq. HCl 2: (i) MeOH, CH2Cl2, (ii) (reduction), (iii) SOCl2 View Scheme
参考文献
Chen,K.S. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 2201 - 2208
反应条件
anhydrous diethylamine hydrochloride; 1,2-diphenyl-2-hydroxyethanone in isopropyl alcohol Further byproducts given;
参考文献
Moore,L.O.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2633 - 2635
反应条件
anhydrous diethylamine hydrochloride; 1,2-diphenyl-2-hydroxyethanone; iron(III) chloride Further byproducts given;
参考文献
Moore,L.O.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2633 - 2635
反应条件
(i) MeOH, CH2Cl2, (ii) (reduction), (iii) SOCl2; Multistep reaction;
参考文献
Chen,K.S. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 2201 - 2208
反应条件
T=95°C; P=73550.8 Torr;
参考文献
Kharasch; Jensen; Urry
Journal of the American Chemical Society, 1947 , vol. 69, p. 1104
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2396261 ;
反应条件
FeIIFe2IIICl8(CH3CN)6 in N,N-dimethyl acetamide; acetonitrile T=130°C; P=15200 Torr; 4 h; other concentrations of CH3CN, DMA; other catalyst; Product distributionMechanism;
参考文献
Lavrent'eva, E. A.; Ponomarev, V. I.; Lavrent'ev, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 12 p. 2534 - 2537
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , vol. 39, # 12 p. 2794 - 2798
