反应条件
1: 1.) diisopropylamine, n-butyllithium; 2.) HMPA / 1.) THF, hexane, 0 deg C, 15 min; 2.) THF, -78 -> 25 deg C, 1.5 h
2: 1.) lithium aluminium hydride; 2.) water, 2 N HCl / 1.) ether, 25 deg C, 30 min; 2.) 30 min
View Scheme
参考文献
Kende, Andrew S.; Newbold, Ronald C.
Tetrahedron Letters, 1989 , vol. 30, # 33 p. 4329 - 4332
