1: With manganese(IV) oxide; 1-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene; 4 A molecular sieve in tetrahydrofuran in situ oxidation-Wittig reaction; 24 h; Heating; 2: With hydrogenchloride in tetrahydrofuran Further stages.;
1: 1.59 g / KF; water / dimethylsulfoxide / 0.75 h 2: 83 percent / water / silver hexafluoroantimonate; (ItBu)AuCl / tetrahydrofuran / 8 h / 60 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 13, # 22 p. 6437 - 6451
