(8ci,9ci)-1H-咪唑并[1,2-a]苯并咪唑合成路线 （共 3 条）
反应条件
1: 99 percent / H2 / 10percent Pd/C / ethanol / 4 h / 2280 Torr / Ambient temperature 2: 1.) 35percent aq. HCl, NaNO2, 2.) aq. NaN3, CH3COONa / 1.) 0 deg C, 2.) r.t., 30 min 3: 12 percent / 500 °C / 0 Torr View Scheme
参考文献
Blake, Alexander J.; Clark, Bernard A. J.; McNab, Hamish; Sommerville, Craig C.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 11 p. 1605 - 1608
反应条件
T=500°C; P=0.0001 Torr;
参考文献
Blake, Alexander J.; Clark, Bernard A. J.; McNab, Hamish; Sommerville, Craig C.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 11 p. 1605 - 1608
反应条件
1: 1.) 35percent aq. HCl, NaNO2, 2.) aq. NaN3, CH3COONa / 1.) 0 deg C, 2.) r.t., 30 min 2: 12 percent / 500 °C / 0 Torr View Scheme
参考文献
Blake, Alexander J.; Clark, Bernard A. J.; McNab, Hamish; Sommerville, Craig C.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 11 p. 1605 - 1608
