6,7-二甲氧基-3,4-二氢-1H-2-萘酮合成路线 （共 28 条）
反应条件
1.1: 100 percent / H2 / 10 percent Pd/C / ethanol / 2585.74 Torr 2.1: KO-tert-Bu / diethyl ether / 0.5 h 2.2: 62 percent / LiCl; HCl; H2O / dimethylsulfoxide / 5 h / 125 °C View Scheme
参考文献
Synthesis, , # 12 p. 2033 - 2035
反应条件
1.1: LDA / tetrahydrofuran / 0.33 h / -78 °C 1.2: tetrahydrofuran / 3 h / -78 - 20 °C 2.1: 74 percent / 1,4-dicyanonaphthalene / acetonitrile; H2O / 4 h / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 9 p. 2867 - 2872
反应条件
1: H2, HClO4 / Pd-C / acetic acid 2: polyphosphoric acid 3: nBuONO, KOtBu / butan-1-ol; diethyl ether 4: Zn / acetic acid 5: NaBH4 6: aq. NaOH / methanol 7: aq. HCl / benzene View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 288 - 293
反应条件
aluminium trichloride in dichloromethane 4 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Medicinal Chemistry, , vol. 25, # 11 p. 1358 - 1363
反应条件
1: 1.) ZnI2; 2.) POCl3 / 2.) pyridine 2: 68 percent / n-Bu4NHSO4, NaOH, H2O2 3: 87 percent / 3N HCl / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 19 p. 3243 - 3246
反应条件
hydrogenchloride in benzene
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 288 - 293
反应条件
2: rhodium(II) acetate / CH2Cl2 / Heating View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 129 - 130
反应条件
1: polyphosphoric acid 2: nBuONO, KOtBu / butan-1-ol; diethyl ether 3: Zn / acetic acid 4: NaBH4 5: aq. NaOH / methanol 6: aq. HCl / benzene View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 288 - 293
反应条件
1: NaBH4 2: aq. NaOH / methanol 3: aq. HCl / benzene View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 288 - 293
反应条件
1: Zn / acetic acid 2: NaBH4 3: aq. NaOH / methanol 4: aq. HCl / benzene View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 288 - 293
