6,7-二甲氧基-3,4-二氢-1H-2-萘酮合成路线 （共 28 条）
反应条件
1: aq. NaOH / methanol 2: aq. HCl / benzene View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 288 - 293
反应条件
1: NaBH4 2: aq. HCl / benzene View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 288 - 293
反应条件
rhodium (II) acetate in dichloromethane Heating; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 129 - 130
反应条件
1: 68 percent / n-Bu4NHSO4, NaOH, H2O2 2: 87 percent / 3N HCl / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 19 p. 3243 - 3246
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / 0 °C 1.2: 73 percent / tetrahydrofuran / 9 h / 0 °C 2.1: 95 percent / DDQ / toluene / Heating 3.1: (CH3)3SnSn(CH3)3 / Pd(PPh3)4 / tetrahydrofuran / Heating 3.2: 120 mg / CuBr / Pd(PPh3)4 / tetrahydrofuran / Heating 4.1: 100 percent / H2 / 10 percent Pd/C / ethyl acetate / 40 - 45 <unit not given> View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 7 p. 1475 - 1491
反应条件
(NH4)2CO3 in ethanol; water T=80°C; 18 h;
参考文献
Obrecht; Spiegler; Schonholzer; Muller; Heimgartner; Stierli
Helvetica Chimica Acta, 1992 , vol. 75, # 5 p. 1666 - 1696
反应条件
sodium azide; methanesulfonic acid T=20°C; Schmidt reaction; 18 h;
参考文献
Dalence-Guzman, Maria F.; Berglund, Magnus; Skogvall, Staffan; Sterner, Olov
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 5 p. 2499 - 2512
反应条件
phosphorus tribromide; bunazosin in N-methyl-acetamide; chloroform; toluene
参考文献
Rutgers, The State University of New Jersey
Patent: US6140328 A1, 2000 ;
