6-甲氧基-3,4-二氢-1H-2-萘酮合成路线 （共 46 条）
反应条件
1: CH2Cl2 2: ZnCl2 / CH2Cl2 3: Zn / acetic acid View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 1 p. 117 - 120
反应条件
hydrogenchloride Heating;
参考文献
Pryde, David C.; Henry, Steven S.; Meyers
Tetrahedron Letters, 1996 , vol. 37, # 19 p. 3243 - 3246
反应条件
1: 95 percent / H2 / platinum / ethanol 2: thionyl chloride / benzene 3: 88 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature 4: 59 percent / diethyl ether / 0.5 h / Ambient temperature 5: 24 percent / acetonitrile / Irradiation View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 458 - 462
反应条件
2: 86 percent / rhodium(II) acetate / CH2Cl2 / Heating View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 129 - 130
反应条件
1: 2N aq. NaOH / 1.) 55 deg C, 2 h, 2.) reflux 2 h 2: 1.) Na, EtOH, 2.) 2N aq. HCl / 1.) reflux, 1 h, 2.) EtOH, reflux, 30 min View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 20 p. 2891 - 2898
反应条件
1: NaBH4 / methanol / 4 h / Ambient temperature 2: 93 percent / oxalic acid / H2O / 6 h / Heating 3: 1.) formic acid, 30 percent hydrogen peroxide; 2.) 20 percent H2SO4 / 1.) 35 deg C, 2 h, room temp., 12 h; 2.) reflux, 10 h View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 5-6 p. 161 - 166
参考文献
Journal of the Chemical Society, , p. 689
反应条件
hydrogenchloride in diethyl ether
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 9, p. 267 - 275
反应条件
sodium carbonate in methanol
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 9, p. 745 - 754
反应条件
1: (i) Na, HOCH2CH2OH, (ii) KHSO4 3: aq. HCl / diethyl ether View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 9, p. 267 - 275
