2-(三苯基正膦基)丙醛合成路线 （共 20 条）
反应条件
in tetrahydrofuran 16 h; Reflux;
参考文献
Bergonzini, Giulia; Vera, Silvia; Melchiorre, Paolo
Angewandte Chemie - International Edition, 2010 , vol. 49, # 50 p. 9685 - 9688
反应条件
in tetrahydrofuran 16 h; Reflux;
参考文献
Bergonzini, Giulia; Vera, Silvia; Melchiorre, Paolo
Angewandte Chemie - International Edition, 2010 , vol. 49, # 50 p. 9685 - 9688
反应条件
NaIO4 on SiO2 in dichloromethane T=20°C;
参考文献
Janthawornpong, Karnjapan; Krasutsky, Sergiy; Chaignon, Philippe; Rohmer, Michel; Poulter, C. Dale; Seemann, Myriam
Journal of the American Chemical Society, 2013 , vol. 135, # 5 p. 1816 - 1822
参考文献
Sloan-Kettering Institute for Cancer Research
Patent: US6369234 B1, 2002 ;
Location in patent: Figure 14A ;
反应条件
in benzene
T=80°C; Wittig reaction; 3 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Keck, Gary E.; Giles, Robert L.; Cee, Victor J.; Wager, Carrie A.; Yu, Tao; Kraft, Matthew B.
Journal of Organic Chemistry, 2008 , vol. 73, # 24 p. 9675 - 9691
参考文献
Sato, Toshio; Hanayama, Kyoko; Fujisawa, Tamotsu
Tetrahedron Letters, 1988 , vol. 29, # 18 p. 2197 - 2200
反应条件
in benzene
T=85°C; 14 h; Heating / reflux;
参考文献
Chelliah, Mariappan V.; Chackalamannil, Samuel; Xia, Yan; Clasby, Martin C.; Greenlee, William J.; Wang, Yuguang; Veltri, Enrico P.; Wu, Wenxue; Graziano, Michael P.; Kosoglou, Teddy; Chintala, Madhu
Patent: US2005/267155 A1, 2005 ;
Location in patent: Page/Page column 13 ;
US 20050267155 A1
反应条件
lead(IV) acetate; sodium hydrogencarbonate
1.) toluene, 4 h, 2.) 18 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Leonard, John; Mohialdin, Soad; Swain, Philip
Synthetic Communications, 1989 , vol. 19, # 20 p. 3529 - 3534
反应条件
sodium hydrogencarbonate in toluene
18 h; in situ trapping of (R)- and (S)-glyceraldehydes by stabilized Wittig Reagents, stereoselectivity; Product distribution;
参考文献
Leonard, John; Mohialdin, Soad; Swain, Philip
Synthetic Communications, 1989 , vol. 19, # 20 p. 3529 - 3534
反应条件
in benzene
T=80°C; 3 h;
参考文献
Parker, Kathlyn A.; Lim, Yeon-Hee
Organic Letters, 2004 , vol. 6, # 2 p. 161 - 164
