10,11-二溴十一烷-1-醇合成路线 （共 13 条）
反应条件
bromine in diethyl ether T=-10 - 0°C; 0.5 h;
参考文献
Narasimhan, S.; Mohan, H.; Madhavan, S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 6 p. 531 - 534
反应条件
sodium tetrahydroborate; iodine in tetrahydrofuran T=25°C; 1 h;
参考文献
Bhanu Prasad; Bhaskar Kanth; Periasamy, Mariappan
Tetrahedron, 1992 , vol. 48, # 22 p. 4623 - 4628
反应条件
N-bromosuccinmide; TBAF*HF in dichloromethane 21 h; Ambient temperature;
参考文献
Camps, F.; Chamorro, E.; Gasol, V.; Guerrero, A.
Journal of Organic Chemistry, 1989 , vol. 54, # 18 p. 4294 - 4298
反应条件
1: 95 percent / lithium aluminum hydride / diethyl ether / 3 h / Heating 2: 100 percent / bromine / diethyl ether / 0.5 h / -10 - 0 °C View Scheme
参考文献
Miyaura, Norio; Suginome, Hiroshi; Suzuki, Akira
Tetrahedron Letters, 1983 , vol. 24, # 14 p. 1527 - 1530
反应条件
bromine; benzo[1,3,2]dioxaborole Yield given. Multistep reaction;
参考文献
Miyaura, Norio; Suginome, Hiroshi; Suzuki, Akira
Tetrahedron Letters, 1983 , vol. 24, # 14 p. 1527 - 1530
反应条件
1: 78 percent / sodium amide / tetrahydrofuran; liquid ammonia / 17 h 2: 62 percent / methanesulfonyl chloride / dimethylformamide; pyridine / 5 h / 1.) 20 deg C to 25 deg C, 5 h; 2.) 75 deg C to 85 deg C, 12 h View Scheme
参考文献
Bishop, Clyde E.; Morrow, Gary W.
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 657 - 660
反应条件
PEG-200; potassium hydroxide 2 h; Heating;
参考文献
Narasimhan, S.; Mohan, H.; Madhavan, S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 6 p. 531 - 534
反应条件
1: NaOMe 2: 1) 1,3,2-benzodioxaborole / 2) Pd(PPh3)4 View Scheme
参考文献
Miyaura, Norio; Suginome, Hiroshi; Suzuki, Akira
Tetrahedron Letters, 1983 , vol. 24, # 14 p. 1527 - 1530
反应条件
1,2-diphenyl-1,2-disodiumethane in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Azzena, Ugo; Pittalis, Mario; Dettori, Giovanna; Madeddu, Simona; Azara, Emanuela
Tetrahedron Letters, 2006 , vol. 47, # 7 p. 1055 - 1058
反应条件
in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Azzena, Ugo; Pittalis, Mario; Dettori, Giovanna; Pisano, Luisa; Azara, Emanuela
Journal of Organometallic Chemistry, 2007 , vol. 692, # 18 p. 3892 - 3900
