3-(3-甲氧基苯基)-1-丙烯合成路线 （共 25 条）
反应条件
ammonia; sodium in ethanol
参考文献
Tyman, John H. P.; Payne
Journal of Chemical Research, 2006 , # 11 p. 691 - 695
反应条件
cesium fluoride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
Suzuki-Miyaura cross-coupling; Heating;
参考文献
Kotha, Sambasivarao; Behera, Manoranjan; Shah, Vrajesh R.
Synlett, 2005 , # 12 art. no. D10405ST, p. 1877 - 1880
反应条件
1: n-propyl-magnesium bromide With zirconocene dichloride in tetrahydrofuran
T=0°C; 0.5 h;
2: With 2,4-dimethylpentan-3-one in tetrahydrofuran
T=25°C; 3 h;
3: 3-methoxy-iodobenzene With triphenylphosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in tetrahydrofuran
T=65°C; 3 h;
参考文献
Hirano, Koji; Fujita, Kazuya; Yorimitsu, Hideki; Oshima, Koichiro
Synlett, 2005 , # 11 art. no. Y00705ST, p. 1787 - 1788
反应条件
tetrakis(triphenylphosphine) palladium(0); lithium chloride in N,N-dimethyl-formamide
T=50°C;
参考文献
Xiao, Qing; Floreancig, Paul E.
Organic Letters, 2008 , vol. 10, # 6 p. 1139 - 1142
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether; water
6 h; Reflux;
参考文献
Nishiwaki, Nagatoshi; Kamimura, Ryuichiro; Shono, Kimihiro; Kawakami, Toshihiko; Nakayama, Katsuhisa; Nishino, Kohei; Nakayama, Takayuki; Takahashi, Keisuke; Nakamura, Aki; Hosokawa, Takahiro
Tetrahedron Letters, 2010 , vol. 51, # 27 p. 3590 - 3592
反应条件
1: 96 percent / triethylamine / CCl4
2: 91 percent / NH3; sodium / ethanol
View Scheme
参考文献
Tyman, John H. P.; Payne
Journal of Chemical Research, 2006 , # 11 p. 691 - 695
参考文献
Tyman, John H. P.; Payne
Journal of Chemical Research, 2006 , # 11 p. 691 - 695
反应条件
1: magnesium; diethyl ether / anschliessendes Behandeln mit wss. Essigsaeure
View Scheme
参考文献
Luettringhaus et al.
Justus Liebigs Annalen der Chemie, 1947 , vol. 557, p. 46,63
参考文献
Luettringhaus et al.
Justus Liebigs Annalen der Chemie, 1947 , vol. 557, p. 46,63
反应条件
1: trichlorophosphate / diethyl ether / |Reflux
2: acetic acid; zinc / 2 h / 0 - 70 °C
3: 3-chloro-benzenecarboperoxoic acid; C39H60N4O4; scandium tris(trifluoromethanesulfonate) / ethyl acetate / 18 h / -60 °C
View Scheme
参考文献
Zhou, Lin; Liu, Xiaohua; Ji, Jie; Zhang, Yuheng; Hu, Xiaolei; Lin, Lili; Feng, Xiaoming
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 20208 - 20208
