N-(苯并咪唑-2-基)-4-氯苯胺合成路线 (共 4 条)
反应条件
(benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=20°C;
参考文献
Wan, Zhao-Kui; Ousman, Erena Farah; Papaioannou, Nikolaos; Saiah, Eddine
Tetrahedron Letters, 2011 , vol. 52, # 32 p. 4149 - 4152
反应条件
potassium dihydrogenphosphate in butan-1-ol T=80°C; 16 h;
参考文献
SANOFI-AVENTIS U.S. LLC; SHAY, John, J., Jr.; CHANDRAMOULI, Sithamalli, V.; LI, XiaoJie; POWERS, Matthew, R.; AYERS, Timothy, A.; HILLEGASS, Andrea
Patent: WO2011/19781 A1, 2011 ;
Location in patent: Page/Page column 9 ;
反应条件
in N,N-dimethyl-formamide T=70°C; 2 h;
参考文献
Xie, Yuanyuan; Zhang, Fan; Li, Jianjun; Shi, Xiangjun
Synlett, 2010 , # 6 p. 901 - 904
反应条件
triethylamine 15 h; Heating;
参考文献
Lan, Ping; Romero, F. Anthony; Malcolm, Threshia S.; Stevens, Benjamin D.; Wodka, Dariusz; Makara, Gergely M.
Tetrahedron Letters, 2008 , vol. 49, # 12 p. 1910 - 1914