2-甲基-2-苯基-1,3-丙烷二醇合成路线 （共 7 条）
反应条件
sodium tetrahydroborate; bromine in ethylene glycol dimethyl ether
T=0 - 20°C; 15 h;
参考文献
Tudge, Matthew; Mashima, Hiroko; Savarin, Cecile; Humphrey, Guy; Davies, Ian
Tetrahedron Letters, 2008 , vol. 49, # 6 p. 1041 - 1044
反应条件
1.1: NaH / dimethylformamide / 0.17 h / 0 °C
1.2: 98 percent / dimethylformamide / 18 h
2.1: 75 percent / LAH / diethyl ether / 18 h / 20 °C
View Scheme
参考文献
Katz, Christopher E.; Aube, Jeffrey
Journal of the American Chemical Society, 2003 , vol. 125, # 46 p. 13948 - 13949
反应条件
pyridine hydrogenfluoride in tetrahydrofuran
T=25°C;
参考文献
Trost, Barry M.; Caldwell, Charles G.
Tetrahedron Letters, 1981 , vol. 22, # 50 p. 4999 - 5002
反应条件
potassium carbonate
T=100°C;
参考文献
Mills; Bains
Journal of the Chemical Society, 1925 , vol. 127, p. 2505
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Testa et al.
Justus Liebigs Annalen der Chemie, 1958 , vol. 619, p. 47,52
Journal of Organic Chemistry, 1959 , vol. 24, p. 1928,1930, 1934
参考文献
Mills; Bains
Journal of the Chemical Society, 1925 , vol. 127, p. 2505
参考文献
Mastagli et al.
Bulletin de la Societe Chimique de France, 1957 , p. 764
