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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
24785-38-4
合成路线
（共 41 条）
696-62-8
4-碘苯甲醚
+
766-97-2
4-甲苯基乙炔
→
反应条件
24785-38-4
反应条件
Cu(acac)2*H2O; potassium carbonate; dimethyl sulfoxide T=140°C; Sonogashira coupling; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Qu, Xiaoming; Xie, Guanlei; Mao, Jincheng
Chemistry - An Asian Journal, 2011 , vol. 6, # 6 p. 1325 - 1330
104-92-7
4-溴苯甲醚
+
624-31-7
4-碘甲苯
+
471-25-0
丙炔酸
→
反应条件
24785-38-4
反应条件
1: 1-(iodo)-4-methylbenzene; acetylenecarboxylic acid With bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=50°C; 4 h; 2: 1-bromo-4-methoxy-benzene in dimethyl sulfoxide T=120°C; 4 h;
参考文献
Lee, Hee Joon; Park, Kyungho; Bae, Goun; Choe, Jaehoon; Song, Kwang Ho; Lee, Sunwoo
Tetrahedron Letters, 2011 , vol. 52, # 39 p. 5064 - 5067
106-38-7
对溴甲苯
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
24785-38-4
反应条件
pyrrolidine; Najera palladacycle I; 4-laurylbenzenesulfonic acid sodium salt; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=130°C; Sonogashira Cross-Coupling; 0.5 h; Microwave irradiationSealed tubeGreen chemistry; chemoselective reaction;
参考文献
Buxaderas, Eduardo; Alonso, Diego A.; Najera, Carmen
European Journal of Organic Chemistry, 2013 , # 26 p. 5864 - 5870
40667-81-0
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
24785-38-4
反应条件
oxygen; palladium diacetate in tetrahydrofuran T=25°C; Sonogashira coupling; P=760.051 Torr; 1.5 h;
参考文献
Pankajakshan, Sreekumar; Loh, Teck-Peng
Chemistry - An Asian Journal, 2011 , vol. 6, # 9 p. 2291 - 2295
104-92-7
4-溴苯甲醚
+
766-97-2
4-甲苯基乙炔
→
反应条件
24785-38-4
反应条件
1-(pyridine-2-yl)-1H-benzo[d][1,2,3]triazole; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=20 - 100°C; Sonogashira Cross-Coupling; 0.25 h; Inert atmosphereSchlenk technique;
参考文献
Verma, Akhilesh K.; Jha, Rajeev R.; Chaudhary, Ritu; Tiwari, Rakesh K.; Danodia, Abhinandan K.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 421 - 438
696-62-8
4-碘苯甲醚
+
2227-58-9
→
反应条件
24785-38-4
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Qu, Xiaoming; Li, Tingyi; Sun, Peng; Zhu, Yan; Yang, Hailong; Mao, Jincheng
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 6938 - 6942
60512-57-4
+
5142-75-6
三对甲苯基铋
→
反应条件
613-33-2
4,4'-二甲基联苯
+
24785-38-4
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=90°C; 2 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
Organic Letters, 2010 , vol. 12, # 9 p. 2048 - 2051
33675-56-8
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
24785-38-4
反应条件
potassium carbonate; palladium dichloride in methanol; water; toluene T=100°C; Sonogashira coupling; 8 h;
参考文献
Shi, Yu; Li, Xiaoyu; Liu, Jianhui; Jiang, Wenfeng; Sun, Licheng
Applied Organometallic Chemistry, 2011 , vol. 25, # 7 p. 514 - 520
5720-05-8
4-甲基苯硼酸
+
61926-37-2
→
反应条件
24785-38-4
反应条件
potassium carbonate; palladium dichloride in methanol; water; toluene T=100°C; Sonogashira coupling; 8 h;
参考文献
Shi, Yu; Li, Xiaoyu; Liu, Jianhui; Jiang, Wenfeng; Sun, Licheng
Applied Organometallic Chemistry, 2011 , vol. 25, # 7 p. 514 - 520
5720-07-0
4-甲氧基苯硼酸
+
766-97-2
4-甲苯基乙炔
→
反应条件
24785-38-4
反应条件
C32H28BrFeIN3Pd; potassium acetate; silver(l) oxide in 1,2-dichloro-ethane T=80°C; 24 h;
参考文献
Li, Hong-Mei; Xu, Chen; Duan, Lu-Meng; Lou, Xin-Hua; Wang, Zhi-Qiang; Li, Zhen; Fan, Yao-Ting
Transition Metal Chemistry, 2013 , vol. 38, # 3 p. 313 - 318
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