1-(4-甲氧基-2-甲基苯基)乙酮合成路线 （共 26 条）
反应条件
1: 64 percent / Br2, aq. NaOH / 0.5 h / 40 °C 2: 73 percent / conc. H2SO4 / 24 h / Heating 3: 73 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 2.5 h / Heating View Scheme
参考文献
Wyrick; Smith; Kemp; Grippo
Journal of Medicinal Chemistry, 1987 , vol. 30, # 10 p. 1798 - 1806
反应条件
[{CpHf(OH2)3}2(μ2-OH)2][OSO2C8F17]4*4H20*2THF in acetonitrile
T=20°C; Friedel Crafts acylation; 6 h; regioselective reaction;
参考文献
Qiu, Renhua; Zhang, Guoping; Zhu, Yuyang; Xu, Xinhua; Shao, Lingling; Li, Yinhui; An, Delie; Yin, Shuangfeng
Chemistry - A European Journal, 2009 , vol. 15, # 26 p. 6488 - 6494
反应条件
potassium carbonate in acetone
Heating;
参考文献
Snider, Barry B.; Zhang, Qingwei
Journal of Organic Chemistry, 1993 , vol. 58, # 11 p. 3185 - 3187
反应条件
zinc trifluoromethanesulfonate in nitromethane
T=20°C; Friedel-Crafts acylation; 8 h;
参考文献
He, Fei; Wu, Huayue; Chen, Jiuxi; Su, Weike
Synthetic Communications, 2008 , vol. 38, # 2 p. 255 - 264
反应条件
1: aluminium chloride
View Scheme
参考文献
v.Auwers; Lechner; Bundesmann
Chemische Berichte, 1925 , vol. 58, p. 41
参考文献
v.Auwers; Lechner; Bundesmann
Chemische Berichte, 1925 , vol. 58, p. 41
反应条件
water; silver trifluoromethanesulfonate
6 h; Heating;
参考文献
Das, Rima; Chakraborty, Debashis
Applied Organometallic Chemistry, 2012 , vol. 26, # 12 p. 722 - 726
反应条件
sodium perchlorate; acetic acid
参考文献
Mathur et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 3582,3585
反应条件
carbon disulfide; aluminium trichloride
参考文献
Noller; Adams
Journal of the American Chemical Society, 1924 , vol. 46, p. 1892
反应条件
1: NaOH
2: 65 percent / SmI3 / acetonitrile / 3 h / 20 °C
View Scheme
参考文献
Chen, Xiaohang; Yu, Mingxin; Wang, Meijun
Journal of Chemical Research, 2005 , # 2 p. 80 - 81
