titanium(IV) isopropylate; (S)-(minus;)-1,1'-bi-2-naphthol in dichloromethane
T=-78 - -20°C; 120.5 h; Molecular sieveInert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Keck, Gary E.; Giles, Robert L.; Cee, Victor J.; Wager, Carrie A.; Yu, Tao; Kraft, Matthew B.
Journal of Organic Chemistry, 2008 , vol. 73, # 24 p. 9675 - 9691
azobisisobutyronitrile in benzene
T=80°C; 3 h; other negatively substituted aliphatic halides, var. tin compounds, reagents, solvents, temp. and time, also with irradiation; Product distribution;
参考文献
Migita; Nagai; Kosugi
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2480 - 2484