2,4-二硝基-1-苯基苯合成路线 （共 22 条）
反应条件
air; tetrabutylammomium bromide; potassium carbonate; [Pd(Cl)κ2N,C,-CH2C6H2(4,6-Me)2CH=NC6H3(2,6-iPr)2]2 in water
Suzuki-Miyaura coupling reaction; 3 h; Heating;
参考文献
Chen, Chuan-Lin; Liu, Yi-Hung; Peng, Shie-Ming; Liu, Shiuh-Tzung
Tetrahedron Letters, 2005 , vol. 46, # 3 p. 521 - 523
反应条件
caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; [((+/-)-BINAP)Pd(MeCN)2](SbF6)2 in ethylene glycol dimethyl ether
T=80°C; Suzuki-Miyaura coupling; 4 h;
参考文献
Mikami, Koichi; Miyamoto, Takashi; Hatano, Manabu
Chemical Communications, 2004 , # 18 p. 2082 - 2083
反应条件
ArPdI(P(C6H5)3)2 in 1,2-dichloro-ethane
T=130°C; 2 h;
参考文献
Kashin, N. A.; Bumagina, I. G.; Bumagin, N. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 1 p. 18 - 24
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 21 - 28
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in acetone
T=20°C; 24 h;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Beletskaya, I. P.
Doklady Chemistry, 1984 , vol. 274, p. 39 - 42
Doklady Akademii Nauk SSSR, 1984 , vol. 274, # 4 p. 818 - 822
反应条件
tetra-(n-butyl)ammonium iodide; (Ph3P)2Pd(Ph)(I) in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=70°C; 3 h;
参考文献
Bumagin, N. A.; Kalinovskii, I. O.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 10 p. 1993
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 10 p. 2413 - 2414
反应条件
{2-[1-(benzyloxyimino)ethyl]benzothiazole-k2N,N'}dichloropalladium(II); tetrabutylammomium bromide; potassium hydroxide in water
T=160°C; Suzuki coupling; 0.0333333 h; Microwave irradiation;
参考文献
Darweesh, Ahmed F.; Shaaban, Mohamed R.; Farag, Ahmad M.; Metz, Peter; Dawood, Kamal M.
Synthesis, 2010 , # 18 p. 3163 - 3173
反应条件
(Ph3P)2Pd(Ph)(I) in 1,2-dichloro-ethane
T=120 - 130°C; 2 h; Yields of byproduct given;
参考文献
Kashin, N. A.; Bumagina, I. G.; Bumagin, N. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 1 p. 18 - 24
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 21 - 28
反应条件
palladium 10 on activated carbon; lithium chloride in 1-methyl-pyrrolidin-2-one
T=120°C; Stille coupling; 24 h;
参考文献
Yabe, Yuki; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2010 , vol. 66, # 45 p. 8654 - 8660
反应条件
dinitrogen trioxide; boron trifluoride
anschliessendes Erwaermen mit Natriumacetat und Acetanhydrid;
参考文献
Bachman; Hokama
Journal of the American Chemical Society, 1957 , vol. 79, p. 4370,4372
反应条件
in 1,2-dichloro-ethane
T=120 - 130°C; 2 h;
参考文献
Kashin, N. A.; Bumagina, I. G.; Bumagin, N. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 1 p. 18 - 24
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 21 - 28
