2,4-二硝基-1-(苯基硫基)苯合成路线 （共 30 条）
反应条件
1: 57 percent / m-CPBA / CH2Cl2 / 2 h 2: 7 percent / hydrogen peroxide; acetic acid / 27 h 3: 100 percent / K2CO3 / dimethylformamide / 0.08 h View Scheme
参考文献
Thompson, Alison; Butler, R. Jonathan; Grundy, Meaghan N.; Laltoo, Andrea B. E.; Robertson, Katherine N.; Cameron, T. Stanley
Journal of Organic Chemistry, 2005 , vol. 70, # 9 p. 3753 - 3756
反应条件
1: 70 percent / CH2Cl2 / 16 h / 20 °C 2: 57 percent / m-CPBA / CH2Cl2 / 2 h 3: 7 percent / hydrogen peroxide; acetic acid / 27 h 4: 100 percent / K2CO3 / dimethylformamide / 0.08 h View Scheme
参考文献
Thompson, Alison; Butler, R. Jonathan; Grundy, Meaghan N.; Laltoo, Andrea B. E.; Robertson, Katherine N.; Cameron, T. Stanley
Journal of Organic Chemistry, 2005 , vol. 70, # 9 p. 3753 - 3756
反应条件
in dichloromethane The mixt. of reagents in CH2Cl2 was stirred overnight;; evapd.;;
参考文献
Cochran, John C.; Bayer, Susan C.; Bilbo, James T.; Brown, Michael S.; Colen, Lawrence B.; at al.
Organometallics, 1982 , vol. 1, p. 586 - 590
反应条件
aluminium trichloride; 1,2-dichloro-ethane
参考文献
Buess; Kharasch
Journal of the American Chemical Society, 1950 , vol. 72, p. 3529,3530
反应条件
1: 7 percent / hydrogen peroxide; acetic acid / 27 h 2: 100 percent / K2CO3 / dimethylformamide / 0.08 h View Scheme
参考文献
Thompson, Alison; Butler, R. Jonathan; Grundy, Meaghan N.; Laltoo, Andrea B. E.; Robertson, Katherine N.; Cameron, T. Stanley
Journal of Organic Chemistry, 2005 , vol. 70, # 9 p. 3753 - 3756
反应条件
1.1: triethylamine / dichloromethane / 0.08 h / 0 °C 1.2: 4 h / 0 - 20 °C 2.1: dimethyl sulfoxide / 0.5 h / pH 7.4 / aq. phosphate buffer View Scheme
参考文献
Sun, Wei; Li, Jing; Li, Wenhua; Su, Lijuan; Du, Lupei; Li, Minyong
Science China Chemistry, 2012 , vol. 55, # 9 p. 1776 - 1780
参考文献
Cullinane et al.
Journal of the Chemical Society, 1936 , p. 1435
Full Text Show Details
Bost; Turner; Norton
Journal of the American Chemical Society, 1932 , vol. 54, p. 1986
Full Text Show Details
Bogert; Evans
Industrial and Engineering Chemistry, 1926 , vol. 18, p. 300
Chem. Zentralbl., 1926 , vol. 97, # I p. 3222
反应条件
sodium sulfide; ethanol anschliessend Umsetzung mit 4-Chlor-1.3-dinitro-benzol in Aethanol;
参考文献
Lukaschewitsch; Ssergejewa
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 1493,1505
Chem.Abstr., 1950 , p. 3451
参考文献
Bielig; Reidies
Chemische Berichte, 1956 , vol. 89, p. 550,561
反应条件
in methanol; water T=25°C; pH 8.00 to 10.00, ionic strength of 0.1 mol l-1; Rate constant;
参考文献
Reeves, W. Preston; Bothwell, Tim C.; Rudis, John A.; McClusky, John V.
Synthetic Communications, 1982 , vol. 12, # 13 p. 1071 - 1079
