hydrogen; palladium on activated charcoal in methanol; acetic acid Ambient temperature;

ethanol; water; hydrazine hydrate

1: triethylamine 2: water; ethanol; N2H4+H2O View Scheme

1: Fmoc-(S)-histidine With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine in 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide Automated synthesizersolid phase reaction; 2: With piperidine in 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide 0.216667 h; Automated synthesizersolid phase reaction; 3: N-(9-fluorenylmethoxycarbonyl)glycine Further stages;

ueber mehrere Stufen;

15K(1+)*H(1+)*25H2O*O122P4W34Zr(16-); water; DCl in water-d2 T=60°C; pH=5;

15K(1+)*H(1+)*25H2O*O122P4W34Zr(16-); water; DCl in water-d2 T=60°C; pH=5;