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乙二醇
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63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-烯丙基萘
合成路线
（共 39 条）
90-14-2
1-碘萘
+
106-95-6
3-溴丙烯
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
1: monoiodonaphthalene With (nBu)3MgLi in tetrahydrofuran; hexane T=-78°C; Metallation; 2: allyl bromide in tetrahydrofuran; hexane T=0°C; Alkylation; 0.5 h;
参考文献
Lee, Kooyeon; Kim, Hyunseok; Mo, Juntae; Lee, Phil Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2147 - 2157
90-11-9
1-溴代萘
+
106-95-6
3-溴丙烯
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
1: 1-Bromonaphthalene With (nBu)3MgLi in tetrahydrofuran; hexane T=-78°C; Metallation; 2: allyl bromide in tetrahydrofuran; hexane T=0°C; Alkylation; 0.5 h;
参考文献
Kitagawa, Kazuya; Inoue, Atsushi; Shinokubo, Hiroshi; Oshima, Koichiro
Angewandte Chemie - International Edition, 2000 , vol. 39, # 14 p. 2481 - 2483
591-87-7
乙酸烯丙酯
+
90-14-2
1-碘萘
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
1: ethylene,methyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 0.5 h; 2: monoiodonaphthalene in N,N-dimethyl-formamide T=100°C; 9 h;
参考文献
Seomoon, Dong; Lee, Kooyeon; Kim, Hyunseok; Lee, Phil Ho
Chemistry - A European Journal, 2007 , vol. 13, # 18 p. 5197 - 5206
556-56-9
丙烯酰碘
+
90-11-9
1-溴代萘
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
indium; triphenylphosphine; lithium chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in N,N-dimethyl-formamide T=100°C; 3 h;
参考文献
Lee, Kooyeon; Kim, Hyunseok; Mo, Juntae; Lee, Phil Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2147 - 2157
556-56-9
丙烯酰碘
+
90-14-2
1-碘萘
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
indium; triphenylphosphine; lithium chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in N,N-dimethyl-formamide T=100°C; 1 h;
参考文献
Lee, Kooyeon; Kim, Hyunseok; Mo, Juntae; Lee, Phil Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2147 - 2157
591-87-7
乙酸烯丙酯
+
99747-74-7
1-萘基三氟甲磺酸酯
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
indium(III) chloride; indium; lithium chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
Seomoon, Dong; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 3 p. 1165 - 1168
556-56-9
丙烯酰碘
+
99747-74-7
1-萘基三氟甲磺酸酯
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
indium; lithium chloride; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=100°C; 1 h;
参考文献
Lee, Kooyeon; Kim, Hyunseok; Mo, Juntae; Lee, Phil Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2147 - 2157
36971-15-0
+
90-11-9
1-溴代萘
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
palladium diacetate; caesium carbonate; tris(4-methylphenyl)-phosphine in toluene 8 h; Heating;
参考文献
Hayashi, Sayuri; Hirano, Koji; Yorimitsu, Hideki; Oshima, Koichiro
Journal of the American Chemical Society, 2006 , vol. 128, # 7 p. 2210 - 2211
1092390-58-3
+
90-11-9
1-溴代萘
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in ethylene glycol dimethyl ether T=85°C; 2 h; Inert atmosphere;
参考文献
Denmark, Scott E.; Werner, Nathan S.
Journal of the American Chemical Society, 2008 , vol. 130, # 48 p. 16382 - 16393
591-87-7
乙酸烯丙酯
+
90-11-9
1-溴代萘
→
反应条件
2489-86-3
1-烯丙基萘
反应条件
1: ethylene,methyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 0.5 h; 2: 1-Bromonaphthalene in N,N-dimethyl-formamide T=100°C;
参考文献
Seomoon, Dong; Lee, Kooyeon; Kim, Hyunseok; Lee, Phil Ho
Chemistry - A European Journal, 2007 , vol. 13, # 18 p. 5197 - 5206
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