2-溴-2′-羟基苯乙酮合成路线 (共 26 条)
反应条件
bromine; acetic acid
参考文献
Buu-Hoi; Lavit
Journal of the Chemical Society, 1955 , p. 18
反应条件
sodium acetate in N,N-dimethyl-formamide 1 h; Heating;
参考文献
Deshpande, A.R.; Paradkar, M.V.
Synthetic Communications, 1990 , vol. 20, # 6 p. 809 - 816
反应条件
1: 88 percent / CH3COONa / dimethylformamide / 1 h / Heating 2: 70 percent / xylene / 40 h / Heating View Scheme
参考文献
Deshpande, A.R.; Paradkar, M.V.
Synthetic Communications, 1990 , vol. 20, # 6 p. 809 - 816
反应条件
β-cyclodextrin in methanol; water T=70°C; 2 h;
参考文献
Madhav; Narayana Murthy; Prakash Reddy; Rama Rao; Nageswar
Tetrahedron Letters, 2009 , vol. 50, # 44 p. 6025 - 6028
反应条件
1: 84 percent / dioxane; ethanol / 1 h / Ambient temperature
2: 93 percent / 3-chloroperoxybenzoic acid / CH2Cl2 / 5 h / 0 °C
3: 60 percent / sodium formate / 70-75 deg C for 3 h then room temperature for 1 h
View Scheme
参考文献
Cremins, Peter J.; Saengchantara, Suthiweth T.; Wallace, Timothy W.
Tetrahedron, 1987 , vol. 43, # 13 p. 3075 - 3082
反应条件
sodium azide in water; acetone
0.5 h;
参考文献
Chowdhury, Nilanjana; Dutta, Sansa; Karthick; Anoop, Anakuthil; Dasgupta, Swagata; Pradeep Singh
Journal of Photochemistry and Photobiology B: Biology, 2012 , vol. 115, p. 25 - 34
反应条件
1: dimethylformamide / 2 h / 40 °C
2: 55 percent / acetic acid / 0.5 h / Heating
View Scheme
参考文献
Cozzi, Paolo; Mongelli, Nicola; Pillan, Antonio
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 311 - 315
反应条件
1: 96 percent / benzene
2: 65 percent / NaOEt / ethanol
View Scheme
参考文献
Shvets, A. A.; Khoruzhaya, I. A.; Kokorev, G. I.; Safaryan, G. P.; Kogan, V. A.
Russian Journal of General Chemistry, 1995 , vol. 65, # 1.1 p. 43 - 45
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 1 p. 53 - 55
反应条件
1: sodium acetate / ethanol
2: ethanol / Acidic conditions; Reflux
View Scheme
参考文献
Shanker, Natasha; Dilek, Ozlem; Mukherjee, Kamalika; McGee, Dennis W.; Bane, Susan L.
Journal of Fluorescence, 2011 , vol. 21, # 6 p. 2173 - 2184
反应条件
1: sodium acetate / ethanol
2: ethanol / Acidic conditions; Reflux
View Scheme
参考文献
Shanker, Natasha; Dilek, Ozlem; Mukherjee, Kamalika; McGee, Dennis W.; Bane, Susan L.
Journal of Fluorescence, 2011 , vol. 21, # 6 p. 2173 - 2184