2-溴-4'-羟基苯乙酮合成路线 （共 52 条）
反应条件
aluminium trichloride; chloroethylmethylchloride
参考文献
US2838570 , ;
US2838570 , ;
反应条件
phenyltrimethylammonium tribromide in methanol; chloroform 0.5 h; other reagent, var. solvents; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 1 p. 295 - 297
反应条件
1: methanol 2: H2; AcOH / Pd/C View Scheme
参考文献
Melgar-Fernandez, Roberto; Demare, Patricia; Hong, Enrique; Rosas, Miguel Angel; Escalante, Jaime; Munoz-Muniz, Omar; Juaristi, Eusebio; Regla, Ignacio
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 1 p. 191 - 194
反应条件
1: methanol 2: H2; AcOH / Pd/C 3: 90 percent / aq. NaOH View Scheme
参考文献
Melgar-Fernandez, Roberto; Demare, Patricia; Hong, Enrique; Rosas, Miguel Angel; Escalante, Jaime; Munoz-Muniz, Omar; Juaristi, Eusebio; Regla, Ignacio
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 1 p. 191 - 194
反应条件
trifluoromethylsulfonic anhydride; NMe4NO3 in dichloromethane 27 h;
参考文献
Shackelford, Scott A.; Anderson, Mark B.; Christie, Lance C.; Goetzen, Thomas; Guzman, Mark C.; Hananel, Martha A.; Kornreich, Wayne D.; Li, Haitao; Pathak, Ved P.; Rabinovich, Alex K.; Rajapakse, Ranjan J.; Truesdale, Larry K.; Tsank, Stella M.; Vazir, Haresh N.
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 267 - 275
反应条件
1: 2-bromo-1-(4-hydroxyphenyl)ethanone With thiamine hydrochloride in ethanol T=20°C; 0.25 h; Green chemistry; 2: 2,4-6-Trihydroxybenzaldehyde in ethanol T=20°C; 1.58333 h; Green chemistry;
参考文献
Mishra, Priya; Singh, Sarita; Ankit, Preyas; Fatma, Shahin; Singh, Divya; Singh, Jagdamba
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 4 p. 1070 - 1076
反应条件
1: 89 percent / p-toluenesulphonic acid / toluene / 4 h / Heating 2: 83.4 percent / NH3 / H2O / 12 h / 50 °C View Scheme
参考文献
Kumar, Ashok; Rane, Ramkrishna A.; Ravindran, Vaikyparambil K.; Dike, Suneel Y.
Synthetic Communications, 1997 , vol. 27, # 7 p. 1133 - 1141
反应条件
toluene-4-sulfonic acid in toluene 4 h; Heating;
参考文献
Kumar, Ashok; Rane, Ramkrishna A.; Ravindran, Vaikyparambil K.; Dike, Suneel Y.
Synthetic Communications, 1997 , vol. 27, # 7 p. 1133 - 1141
反应条件
1: With 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in chloroform T=20°C; 1 h; 2: With hydrogenchloride in ethanol T=20°C; 1 h; Further stages.;
参考文献
Xue, Na; Yang, Xiaochun; Wu, Rui; Chen, Jing; He, Qiaojun; Yang, Bo; Lu, Xiuyang; Hu, Yongzhou
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 5 p. 2550 - 2557
反应条件
DMBI in tetrahydrofuran 3 h; Heating;
参考文献
Chikashita, Hidenori; Ide, Hisao; Itoh, Kazuyoshi
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5400 - 5405
