2-溴-4'-羟基苯乙酮合成路线 (共 52 条)
反应条件
hydrogen; palladium 10 on activated carbon in methanol 10 h;
参考文献
Purohit, Ajay; Casebier, David S.
Patent: US2006/83681 A1, 2006 ;
Location in patent: Page/Page column 11 ;
反应条件
1: 87 percent / dimethylformamide / 50 °C 2: 0.5 h / Photolysis View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 10 p. 2453 - 2463
反应条件
1: DBU / benzene 2: TFA 3: H2O / 25 °C / Irradiation; buffer View Scheme
参考文献
Givens; Jung; Park; Weber; Bartlett
Journal of the American Chemical Society, 1997 , vol. 119, # 35 p. 8369 - 8370
反应条件
sodium azide in N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
Edegger, Klaus; Gruber, Christian C.; Poessl, Tina M.; Wallner, Sabine R.; Lavandera, Ivan; Faber, Kurt; Niehaus, Frank; Eck, Juergen; Oehrlein, Reinhold; Hafner, Andreas; Kroutil, Wolfgang
Chemical Communications, 2006 , # 22 p. 2402 - 2404
参考文献
Hashimoto; Ohta
Nippon Kagaku Zasshi, 1959 , vol. 80, p. 212
Chem.Abstr., 1961 , p. 4406
反应条件
potassium carbonate in acetone
Thorpe-Zigler cyclization; Heating;
参考文献
Mahadevan; Vaidya; Vagdevi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 8 p. 1931 - 1936
反应条件
1: 85 percent / potassium carbonate / acetone / Heating
2: 60 percent / hydroxylamine hydrochloride; aqueous potassium hydroxide / ethanol / Heating
View Scheme
参考文献
Mahadevan; Vaidya; Vagdevi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 8 p. 1931 - 1936
反应条件
1: 85 percent / potassium carbonate / acetone / Heating
2: 50 percent / aqueous sodium hydroxide / 20 °C
View Scheme
参考文献
Mahadevan; Vaidya; Vagdevi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 8 p. 1931 - 1936
反应条件
1: 85 percent / potassium carbonate / acetone / Heating
2: 60 percent / aqueous sodium hydroxide / 20 °C
View Scheme
参考文献
Mahadevan; Vaidya; Vagdevi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 8 p. 1931 - 1936
反应条件
ethanol
und Erhitzen des Reaktionsprodukts mit wss. Natriumhydrogencarbonat-Loesung;
参考文献
Buu-Hoi et al.
Journal of the Chemical Society, 1954 , p. 1034,1037