4-硝基-4-二甲基氨基偶氮苯合成路线 (共 38 条)
反应条件
in acetonitrile Ambient temperature;
参考文献
Sheinkman, A. K.; Skorobogatova, Z. M.; Chmilenko, T. S.; Baranova, T. M.
Doklady Chemistry, 1982 , vol. 267, p. 428 - 431
Dokl. Akad. Nauk SSSR Ser. Khim., 1982 , vol. 267, # 2 p. 405 - 409
反应条件
in tetrahydrofuran T=-20°C; 1 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 26, # 3.2 p. 522 - 527
Zhurnal Organicheskoi Khimii, , vol. 26, # 3 p. 610 - 616
反应条件
in sulfuric acid; acetic acid T=0°C; 1.5 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 1641 - 1646
Zhurnal Organicheskoi Khimii, , vol. 16, # 9 p. 1927 - 1933
反应条件
1: 86 percent / ethanol; H2O / 6 h / 8 °C 2: 30 percent / ethanol; H2O / 3 h / 8 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 455 - 460
反应条件
hydrogenchloride; sodium acetate
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 947 - 953
Zhurnal Organicheskoi Khimii, , vol. 22, # 5 p. 1054 - 1061
参考文献
Chemische Berichte, , vol. 28, p. 830
Chemische Berichte, , vol. 30, p. 216 Anm.4
参考文献
Journal of the Chemical Society, , vol. 45, p. 116
反应条件
1: 86 percent / ethanol; H2O / 6 h / 8 °C 2: 30 percent / ethanol; H2O / 3 h / 8 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 455 - 460
反应条件
1: 75 percent / ethanol; H2O / 6 h / 8 °C 2: 30 percent / ethanol; H2O / 3 h / 8 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 455 - 460
参考文献
Monatshefte fuer Chemie, , vol. 84, p. 610,617