4-硝基苯-Β-D-吡喃葡萄糖苷合成路线 （共 51 条）
反应条件
Thermus nonproteolyticus HG102 E338A mutant; glycine; sodium hydroxide in aq. buffer T=45°C; pH=8.8; 48 h; Enzymatic reaction; Overall yield = 90 percent;
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
AbgGlu358Ala; ammonium bicarbonate buffer 8 h; Ambient temperature;
参考文献
Mackenzie; Wang; Antony; Warren; Withers
Journal of the American Chemical Society, 1998 , vol. 120, # 22 p. 5583 - 5584
反应条件
β-D-galactosidase from Bacillus circulans in water; acetonitrile 1.) phosphate buffer pH 7.0, 40 deg C, 6 h, 2.) 95 deg C, 10 min.; Yield given. Yields of byproduct given;
参考文献
Murata; Akimoto; Horimoto; Usui
Bioscience, biotechnology, and biochemistry, 1997 , vol. 61, # 7 p. 1118 - 1120
反应条件
β4galT; manganese (II) chloride; bovine serum albumin in various solvent(s) T=37°C; pH=7.5; Enzymatic reaction; Product distribution; Further Variations:Reagents;
参考文献
Blixt; Brown; Schur; Wakarchuk; Paulson
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2442 - 2448
反应条件
phosphate buffer; β-glucosidase T=30°C; 26 h;
参考文献
Akita, Hiroyuki; Kurashima, Katsumi; Nakamura, Takuya; Kato, Keisuke
Tetrahedron Asymmetry, 1999 , vol. 10, # 12 p. 2429 - 2439
反应条件
β-D-glycosidase from Thermus thermophilus in N,N-dimethyl-formamide T=30°C; pH=7; 2 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Marton, Zsuzanna; Tran, Vinh; Tellier, Charles; Dion, Michel; Drone, Jullien; Rabiller, Claude
Carbohydrate Research, 2008 , vol. 343, # 17 p. 2939 - 2946
反应条件
AbgGlu358Ala; ammonium bicarbonate buffer 8 h; Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 120, # 22 p. 5583 - 5584
反应条件
1: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction 2: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
phosphate buffer; β-glucosidase T=30°C; pH=5; 24 h;
参考文献
Kurashima, Katsumi; Fujii, Mikio; Ida, Yoshiteru; Akita, Hiroyuki
Chemical and Pharmaceutical Bulletin, 2004 , vol. 52, # 2 p. 270 - 275
反应条件
1: 25 percent / β-glucosidase, phosphate buffer, pH 5 / 24 h / 30 °C 2: 98 percent / pyridine, 4-dimethylaminopyridine / 0.25 h / Ambient temperature 3: 1.) O3, 2.) Me2S / 1.) CH2Cl2, -78 deg C, 2 h, 2.) CH2Cl2, RT, 30 min 4: 1.) NaH / 1.) n-hexane, THF, 0 deg C, 15 min, 2.) n-hexane, THF, 0 deg C, 30 min 5: 77 percent / K2CO3 / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Akita, Hiroyuki; Kurashima, Katsumi; Nakamura, Takuya; Kato, Keisuke
Tetrahedron Asymmetry, 1999 , vol. 10, # 12 p. 2429 - 2439
