2,4,6-三叔丁基亚硝基苯合成路线 （共 14 条）
反应条件
lt;CpW(CO)3gt;2 in benzene
T=20°C; Irradiationrate constant for CpW(CO)3 radical addition, other reactant: CpW(CO)3Me; Rate constant;
参考文献
Gasanov, R.G.; Freidlina, R.Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2409 - 2411
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2631 - 2633
参考文献
Inagaki,Y. et al.
Bulletin of the Chemical Society of Japan, 1975 , vol. 48, p. 621 - 625
反应条件
in toluene
T=-80 - -25°C; 2 h; or in ethyl acetate; Product distributionMechanism;
参考文献
Florjanczyk, Zbigniew; Langwald, Norbert
Journal of Organometallic Chemistry, 1986 , vol. 312, p. 297 - 304
反应条件
hydrogenchloride in tetrahydrofuran; diethyl ether
inert atmosphere; addn. of org. compd. soln. (THF) to soln. of Ge-compd. (THF/Et2O) at -20°C, keeping at same temp. for 30 min, at room temp. for 1 h, soln. hydrolysis; twice extn. (Et2O), drying (Na2SO4), soln. concn. (reduced pressure); (1)H-NMR and ESR spectroscopy;
参考文献
Riviere, P.; Castel, A.; Desor, D.; Abdennadher, C.
Journal of Organometallic Chemistry, 1993 , vol. 443, # 1 p. 51 - 60
