5-对甲苯基-1H-四氮唑合成路线 （共 26 条）
反应条件
1: With sodium azide in N,N-dimethyl-formamide T=120°C; 36 h; 2: With hydrogenchloride in water; ethyl acetate 0.0833333 h;
参考文献
Lang, Leiming; Li, Baojun; Liu, Wei; Jiang, Li; Xu, Zheng; Yin, Gui
Chemical Communications, 2010 , vol. 46, # 3 p. 448 - 450
反应条件
sodium azide; copper diacetate in N,N-dimethyl-formamide T=120°C; 12 h;
参考文献
Patil, Umakant B.; Kumthekar, Kedar R.; Nagarkar, Jayashree M.
Tetrahedron Letters, 2012 , vol. 53, # 29 p. 3706 - 3709
反应条件
sodium azide; copper ferrite in N,N-dimethyl-formamide T=120°C; 12 h; Sealed tube;
参考文献
Akula, Ravi Kumar; Adimulam, Chandra S.; Gangaram, Sathaiah; Kengiri, Raju; Banda, Narsaiah; Pamulaparthy, Shanthan R.
Letters in Organic Chemistry, 2014 , vol. 11, # 6 p. 440 - 445
反应条件
[bmim][N3]; hydroxylamine; copper diacetate in N,N-dimethyl-formamide T=120°C; 12 h;
参考文献
Heravi, Majid M.; Fazeli, Azadeh; Oskooie, Hossein A.; Beheshtiha, Yahya S.; Valizadeh, Hassan
Synlett, 2012 , vol. 23, # 20 p. 2927 - 2930
反应条件
sodium azide; tetrachlorosilane in acetonitrile T=20 - 82°C; 1.66667 h;
参考文献
El-Ahl, Abdel-Aziz S.; Amer, Fatty A.; Elbeheery, Akram H.
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 11 p. 2226 - 2235
反应条件
triazidochlorosilane in acetonitrile 2 h; Heating;
参考文献
El-Ahl, Abdel-Aziz S.; Elmorsy, Saad S.; Elbeheery, Akram H.; Amer, Fathy A.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1257 - 1260
反应条件
1,4-diaza-bicyclo[2.2.2]octane; sodium azide; palladium diacetate; sodium carbonate; zinc dibromide in N,N-dimethyl-formamide T=140°C; 24 h; Inert atmosphere;
参考文献
Zhu, Yizhong; Ren, Yiming; Cai, Chun
Helvetica Chimica Acta, 2009 , vol. 92, # 1 p. 171 - 175
反应条件
1: 90 percent / Pd(PPh3)4 / dimethylformamide / 0.03 h / microwave irradiation 2: 91 percent / NaN3; NH4Cl / dimethylformamide / 0.25 h / microwave irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 23 p. 7984 - 7989
反应条件
1: CuO / N,N-dimethyl-formamide / 100 °C 2: CuO; sodium azide / N,N-dimethyl-formamide View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 35 p. 4732 - 4734
反应条件
acetic acid; sodium nitrite
参考文献
Justus Liebigs Annalen der Chemie, , vol. 298, p. 30
Chemische Berichte, , vol. 27, p. 3279
